Preparation method of high-light-transmittance amphiphobic antireflection film
A technology of anti-reflection film and high light transmittance, applied in the direction of coating, etc., can solve the problems of low solid/liquid adhesion and high transparency
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Embodiment 1
[0025] (1) Aluminum nitrate is dissolved in 2-isopropoxyethanol, and then ethanolamine is added dropwise as a stabilizer. The resulting solution was stirred at room temperature for 1 hour to form a transparent aluminum sol;
[0026] Wherein, the mol ratio of aluminum nitrate and 2-isopropoxyethanol is 1:17, and the volume addition of ethanolamine is 3% of the volume addition of 2-isopropoxyethanol;
[0027] With ethanol (EtOH) as solvent, ammonia (NH 4 OH) as a catalyst, and tetraethyl orthosilicate (TEOS) as a silicon source, 20nm SiO was prepared by sol-gel method 2 Solid pellet sol;
[0028] Among them, EtOH, TEOS and NH 4 The molar ratio of OH is 114:3:5.4;
[0029] (2) 20nm SiO 2 Sol and Al 2 o 3 The sol is mixed at a mass ratio of 1:1 and dispersed ultrasonically to obtain uniform and stable SiO 2- al 2 o 3 Mixed sol.
[0030] (3) The dipping-pulling method is used to plate the coating, the pulling speed of the plated coating is 60mm / min, and the dipping time ...
Embodiment 2
[0033] Aluminum sol and SiO 2 The preparation of the solid bead sol is the same as in Example 1.
[0034] (1) 20nm SiO 2 Sol and Al 2 o 3 The sol is mixed at a mass ratio of 1:2 and dispersed ultrasonically to obtain uniform and stable SiO 2- al 2 o 3 Mixed sol.
[0035](2) The dipping-pulling method is used to plate the coating, the pulling speed of the plated coating is 60mm / min, and the dipping time is 360s. After the coated substrate was immediately cured at 100 °C for 5 min, it was calcined in a muffle furnace at 400 °C for 1 h to obtain Al 2 o 3 -SiO 2 membrane, and then immersed in deionized water at 90°C for 30 minutes to obtain a hydrophilic and lipophilic anti-reflective membrane.
[0036] (3) Put the plated film layer into a vacuum desiccator, drop 500 μL PFDTES into it, deposit it for 48 hours, and then put it into a 180° C. oven for curing for 30 minutes to prepare a double thinning anti-reflection film. The highest light transmittance of the coating is...
Embodiment 3
[0038] Aluminum sol and SiO 2 The preparation of the solid bead sol is the same as in Example 1.
[0039] (1) 20nm SiO 2 Sol and Al 2 o 3 The sol is mixed with a mass ratio of 1:3 and dispersed ultrasonically to obtain uniform and stable SiO 2- al 2 o 3 Mixed sol.
[0040] (2) The dipping-pulling method is used to plate the coating, the pulling speed of the plated coating is 60mm / min, and the dipping time is 360s. After the coated substrate was immediately cured at 100 °C for 5 min, it was calcined in a muffle furnace at 400 °C for 1 h to obtain Al 2 o 3 -SiO 2 membrane, and then immersed in deionized water at 90°C for 30 minutes to obtain a hydrophilic and lipophilic anti-reflective membrane.
[0041] (3) Put the plated film layer into a vacuum desiccator, drop 500 μL PFDTES into it, deposit it for 48 hours, and then put it into a 180° C. oven for curing for 30 minutes to prepare a double thinning anti-reflection film. The highest light transmittance of the coating...
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