Pb<2+> concentration detection sensor and device, preparation method and use method
A concentration detection and sensor technology, applied in the field of pb2+ concentration detection, can solve the problems of low detection selectivity and high price, and achieve the effect of high detection selectivity and low cost
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[0088] Dilute the 36% acetic acid solution with deionized water to 4% by mass. Dissolve 100mg chitosan in 10ml 4% acetic acid solution. Stir continuously at 100° C. for 2 hours with a magnetic stirrer to obtain a 1 wt % chitosan solution. Dilute the 35% polyacrylic acid to 10% with deionized water.
[0089] A section of photonic crystal fiber 102 with a length of 2 cm is fused between two standard single-mode fibers 101 as a sensing element. The sensor was then soaked in piranha solution (70% sulfuric acid and 30% hydrogen peroxide) for 60 minutes to remove organic impurities on its surface, then rinsed with deionized water several times, and finally dried in an oven.
[0090] Place the sensing element in the chitosan solution for 5 minutes, dry it in the air for 1 minute, then soak it in deionized water for 1 minute to wash off the chitosan with weak surface binding ability, and then place it in the polyacrylic acid solution for reaction 5 minutes, and 1 minute in dry air,...
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