Pigment dispersant and pigment dispersion composition
A technology of dispersant and pigment, which is applied in the direction of pigment slurry, dyeing polymer organic compound treatment, pigment-containing coating, etc., and can solve the problems of low initial viscosity, thickening, and high initial viscosity of inorganic pigment slurry
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Embodiment 1
[0078] Put 420 parts of isopropanol and 120 parts of water into a pressure-resistant reaction vessel, replace it with nitrogen, seal it, and raise the temperature to 100°C. Under stirring, at the same temperature, mix a homogeneous mixture of 305 parts of acrylic acid, 5 parts of triethylene glycol dithiol, 1 part of ascorbic acid, 50 parts of isopropanol and 50 parts of water, and 50 parts of 5% aqueous hydrogen peroxide , taking 3.5 hours to drip from their respective containers. After the dropwise addition was terminated, 3 parts of 35% hydrogen peroxide aqueous solution was added, and the temperature was kept at the same temperature for 1 hour to obtain a polymer (a) with a polymerization rate of 99.9%. The weight-average molecular weight measured by GPC is 11500, the maximum peak molecular weight (M) is 10 000, and the low molecular weight polymer content (M×0.2=2000, area % of molecular weight less than 2000 in GPC) is 0.7%. After neutralizing with 339 parts of a 30% aq...
Embodiment 2、3、4
[0080] Except that the neutralization salt and the degree of neutralization of the polymer (a) used were replaced with those recorded in Table 1, the rest were operated in the same manner as in Example 1 to obtain a polyacrylate salt solution.
Embodiment 5
[0082] 420 parts of isopropanol and 120 parts of water were placed in a pressure-resistant reaction vessel, and after replacing with nitrogen, it was sealed and heated to 100°C. Under stirring, 305 parts of acrylic acid and 80 parts of a 4% aqueous solution of sodium persulfate were dropped from respective containers over 3 hours. After the dropwise addition was terminated, 3 parts of 35% hydrogen peroxide aqueous solution was added, and the temperature was kept at the same temperature for 1 hour to obtain a polymer (b) with a polymerization rate of 99.8%. Its weight-average molecular weight measured by GPC is 9200, the maximum peak molecular weight (M) is 9000, and the low-molecular-weight polymer content (M×0.2=1800, the area percent of molecular weight in GPC less than 1800) is 3.6%. Neutralize with 395 parts of a 30% aqueous solution of sodium hydroxide, 12.8 parts of adducts of 2 moles of propylene oxide of dodecylamine, and distill off isopropanol to obtain polyacrylic a...
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