A kind of metal roof waterproof coating and preparation method thereof
A technology for waterproof coatings and metal roofs, which is applied in the direction of coatings, etc., can solve the problems of affecting the service life of waterproof effects, poor low-temperature flexibility of waterproof coatings, and difficulty in adapting coatings to metal roofs, etc., to achieve improved storage stability, good weather resistance, and extended The effect of service life
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preparation example 1
[0037] Preparation Example 1 of Polymer Emulsion: ① Preparation of Polyurethane Prepolymer: Take 2kg of isophorone diisocyanate and 6kg of polyoxypropylene glycol, add 0.2kg of ethylene glycol chain extender and 0.01kg of dibutyltin dilaurate The catalyst was reacted at a temperature of 70 ° C for 2 hours, then 0.4 kg of sodium 1,2-dihydroxy-3-propanesulfonate was added, and the reaction was continued until the NCO content remained unchanged to obtain a polyurethane prepolymer;
[0038] ②Preparation of pre-emulsion: take 3kg of butyl acrylate, 4kg of methyl acrylate, 3kg of n-octyl acrylate, 0.6kg of sodium lauryl sulfate, 0.2kg of nonylphenol polyoxyethylene ether, 0.2kg of dodecylene Sodium propyl succinate alkyl sulfonate, 0.3kg N-methylol acrylamide, 0.1kg ammonium persulfate and 100kg deionized water, stir and heat up to 85°C, keep stirring for 10min, then add 0.5kg polyether acrylate, 0.2 kg of polyethylene glycol monomethyl ether and 0.2 kg of polycaprolactone were stir...
preparation example 2
[0040] Preparation example 2 of polymer emulsion: ① Preparation of polyurethane prepolymer: take 2.5kg isophorone diisocyanate and 7kg polyoxypropylene glycol, add 0.3kg ethylene glycol chain extender and 0.015kg dilauric acid diol The butyltin catalyst was reacted at a temperature of 75°C for 2.5h, then 0.5kg of sodium 1,2-dihydroxy-3-propanesulfonate was added, and the reaction was continued until the NCO content remained unchanged to obtain a polyurethane prepolymer;
[0041] ②Preparation of pre-emulsion: take 3.75kg butyl acrylate, 5kg methyl acrylate, 3.75kg n-octyl acrylate, 0.9gkg sodium lauryl sulfate, 0.3kg nonylphenol polyoxyethylene ether, 0.3kg dodecane Alkyl allyl succinate sodium sulfonate, 0.45kg N-methylol acrylamide, 0.15kg sodium persulfate and 100kg deionized water, stir and heat up to 88°C, keep stirring for 12min, then add 0.75kg polyether acrylic acid Ester, 0.3kg polyethylene glycol monomethyl ether and 0.3kg polycaprolactone were kept at a temperature o...
preparation example 3
[0043] Preparation Example 3 of Polymer Emulsion: 1. Preparation of Polyurethane Prepolymer: Take 3kg of isophorone diisocyanate and 8kg of polyoxypropylene glycol, add 0.4kg of ethylene glycol chain extender and 0.02kg of dibutyltin dilaurate The catalyst was reacted at a temperature of 80 ° C for 3 hours, then 0.6 kg of sodium 1,2-dihydroxy-3-propanesulfonate was added, and the reaction was continued until the NCO content remained unchanged to obtain a polyurethane prepolymer;
[0044] ②Preparation of pre-emulsion: take 4.5kg butyl acrylate, 6kg methyl acrylate, 4.5kg n-octyl acrylate, 1.2kg sodium lauryl sulfate, 0.4kg nonylphenol polyoxyethylene ether, 0.4kg dodecane Alkyl allyl succinate sodium sulfonate, 0.5kg N-methylol acrylamide, 0.2kg potassium persulfate and 100kg deionized water, stir and heat up to 90°C, keep stirring for 15min, then add 0.8kg polyether acrylic acid Esters, 0.4kg polyethylene glycol monomethyl ether and 0.4kg polycaprolactone were kept at a temper...
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