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Multifunctional liquid soap containing amino propanesulfonic acid inner salt structure, and preparation method for multifunctional liquid soap

An aminopropanesulfonic acid and multi-functional technology, which is applied in the field of detergents, can solve the problems of small cationic quaternary ammonium salt molecules, can not meet the requirements of use, and short hand contact time, so as to improve the ecological degradable effect and improve sterilization and disinfection. effect, the effect of reducing instability

Pending Publication Date: 2020-06-26
SHAANXI UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, these cationic quaternary ammonium salts have small molecules, are easy to lose, and have short contact time with hands
Furthermore, quaternary ammonium cations have certain irritation and cannot meet the requirements for use as cleaning products such as cleaning human skin.

Method used

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  • Multifunctional liquid soap containing amino propanesulfonic acid inner salt structure, and preparation method for multifunctional liquid soap
  • Multifunctional liquid soap containing amino propanesulfonic acid inner salt structure, and preparation method for multifunctional liquid soap
  • Multifunctional liquid soap containing amino propanesulfonic acid inner salt structure, and preparation method for multifunctional liquid soap

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preparation example Construction

[0034] The preparation method of the multifunctional hand sanitizer containing aminopropanesulfonic acid internal salt formula amphoteric structure of the present invention specifically comprises the following steps:

[0035] Step 1: Mix 20-25 parts of starch with 100-130 parts of deionized water and 0.2-0.3 parts of high-temperature α-amylase according to parts by weight, heat to 90°C-95°C, keep warm for 2.5-3.5 hours to perform degradation reaction, and obtain Degraded starch solution;

[0036]Step 2: Add 10 to 12 parts of N,N-dimethyl (methacryloyloxyethyl) aminopropanesulfonic acid inner salt and 6 to 8 parts of acrylamide to the above degraded starch solution, stir and heat to 40 At ~45°C, add 4 to 6 parts of buffer solution to adjust the pH value of the system to 6.3 to 6.5, and at the same time add 5 to 8 parts of horseradish peroxidase solution with a mass fraction of 0.09% to 0.15% and a mass fraction of 30% 8 to 10 parts of hydrogen peroxide solution, and the droppi...

Embodiment 1

[0058] Step 1. Mix 20 parts of starch with 100 parts of deionized water and 0.2 parts of high-temperature α-amylase in parts by mass, heat to 90° C., and keep warm for 2.5 hours for degradation reaction to obtain a degraded starch solution;

[0059] Step 2. Add 10 parts of N,N-dimethyl(methacryloyloxyethyl)aminopropanesulfonic acid inner salt and 6 parts of acrylamide to the above degraded starch solution, stir and heat to 40°C, add buffer 4 parts of the solution to adjust the pH value of the system to 6.3, while 5 parts of horseradish peroxidase solution with a mass fraction of 0.09% and 8 parts of a hydrogen peroxide solution with a mass fraction of 30% were added dropwise, and the dropping time was controlled to be 2.0 hours After the dropwise addition is completed, continue the heat preservation reaction for 4.5 hours to obtain the modified starch;

[0060] Step 3: Add 25 parts of polyether macromonomer, 15 parts of N,N-dimethyl (methacryloyloxyethyl) aminopropanesulfonic ...

Embodiment 2

[0067] Step 1. Mix 23 parts of starch with 120 parts of deionized water and 0.25 parts of high-temperature α-amylase in parts by mass, heat to 95° C., and keep warm for 3.5 hours for degradation reaction to obtain a degraded starch solution;

[0068] Step 2. Add 12 parts of N,N-dimethyl(methacryloyloxyethyl) aminopropanesulfonic acid inner salt and 8 parts of acrylamide to the above degraded starch solution, stir and heat to 45°C, add buffer 6 parts of the solution to adjust the pH value of the system to 6.5, while 7 parts of the horseradish peroxidase solution with a mass fraction of 0.12% and 9 parts of a hydrogen peroxide solution with a mass fraction of 30% were added dropwise, and the dropping time was controlled to be 2.5 hours , after the dropwise addition, continue the heat preservation reaction for 5.5 hours to obtain the modified starch;

[0069] Step 3: Add 30 parts of polyether macromonomer, 18 parts of N,N-dimethyl (methacryloyloxyethyl) aminopropanesulfonic acid ...

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Abstract

The invention discloses a multifunctional liquid soap containing an amino propanesulfonic acid inner salt structure, and a preparation method for the multifunctional liquid soap. The preparation method comprises the following steps of: firstly, carrying out enzymatic degradation on starch to prepare degrading starch; under a function of horseradish peroxidase, carrying out modified starch graftingby 3-[ Dimethyl- [ 2-(2-methylprop-2-enoyloxy) ethyl ] azaniumyl ] propane-1-sulfonate; then, preparing a copolymer of acrylic acid, the 3-[ Dimethyl- [ 2-(2-methylprop-2-enoyloxy) ethyl ] azaniumyl] propane-1-sulfonate and allyl alcohol ethoxylate; enabling animal oleic acid to react with methoxypolyethylene glycol to react to prepare animal oleic acid methoxypolyethylene glycol ester; and compounding the prepared grafted modified starch, copolymer and animal oleic acid methoxypolyethylene glycol ester with lauryl sodium sulfate, acrylic acid, sodium methallyl sulfonate, sodium tripolyphosphate, triterpenoid saponin, isothiazolinone, citric acid, essences, pigments and the like to prepare an ecological liquid soap containing the amino propanesulfonic acid inner salt structure. The product is friendly to environment, exhibits small irritation on the skin of the human body and the like, has powerful sterilization and detergency and has high cost performance.

Description

technical field [0001] The invention relates to detergents, in particular to a multifunctional hand sanitizer containing aminopropanesulfonic acid internal salt amphoteric structure and a preparation method thereof. Background technique [0002] Washing your hands frequently and knowing how to wash your hands is the most effective, simplest and feasible way to control the spread of diseases and prevent infection. It has a good preventive effect on diseases transmitted by the digestive tract and diseases transmitted by the respiratory tract. The SARS epidemic in 2003 made people generally improve their self-protection awareness in daily life. The most common self-protection habit is to wash their hands frequently and know how to wash their hands. The spread of the new crown pneumonia epidemic that began around the Spring Festival in 2020 is another reminder People should start from their daily habits to improve their awareness and behavior of self-protection. Washing hands fr...

Claims

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Application Information

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IPC IPC(8): A61K8/81A61K8/73A61K8/85A61K8/86A61K8/04A61Q19/10A61Q19/00A61Q17/00C08F283/06C08G65/332C08F251/00C08F220/38C08F220/06
CPCA61K8/8147A61Q19/10A61Q17/005A61Q19/00A61K8/732A61K8/86A61K8/85A61K8/046C08F283/065C08G65/3322C08F251/00A61K2800/5426A61K2800/805C08F220/06Y02A50/30
Inventor 吕生华刘相高惠侠杨俊杰李宁国郭子轶杨震
Owner SHAANXI UNIV OF SCI & TECH
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