Preparation method of metal oxide composite magnesium hydride hydrogen storage material
A technology for composite magnesium hydride and hydrogen storage materials, which is applied in the field of preparation of metal oxide composite magnesium hydride hydrogen storage materials, can solve the problems that the hydrogen desorption performance of MgH2 does not show improvement, and achieve significant kinetic performance, eliminate agglomeration, and composition reasonable effect
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Embodiment 1
[0015] The preparation method of the metal oxide composite magnesium hydride hydrogen storage material is as follows: using magnesium hydride as a base material, mixing metal oxide particles, the mass percentage of each component in the mixture is: magnesium hydride 99%, α- Fe 2 o 3 1%; the mixture is charged with hydrogen in a ball mill, and charged with hydrogen (0.4MPa) in a planetary ball mill for 80h, the ball-to-material ratio is 20:1, and the ball milling speed is 180r / min, and the obtained metal oxide is compositely hydrogenated The particle size of the magnesium hydrogen storage material is 28.0-60.0nm.
[0016] The hydrolysis rate of the obtained composite magnesium hydride hydrogen storage material increases significantly with the increase of temperature. At a normal temperature of 25°C, the composite magnesium hydride hydrogen storage material is hydrolyzed in twice distilled water for 15 minutes to release hydrogen gas of 65% of the theoretical hydrogen storage ...
Embodiment 2
[0018] The preparation method of the metal oxide composite magnesium hydride hydrogen storage material is as follows: using magnesium hydride as a base material, mixing metal oxide particles, the mass percentage of each component in the mixture is: magnesium hydride 98%, TiO 2 2%; the mixed material is charged with hydrogen in a ball mill, and charged with hydrogen (0.4MPa) in a planetary ball mill for 80h, the ball-to-material ratio is 20:1, and the ball milling speed is 180r / min, and the obtained metal oxide is compositely hydrogenated The particle size of the magnesium hydrogen storage material is 28.0-60.0nm.
[0019] The hydrolysis rate of the obtained composite magnesium hydride hydrogen storage material increases significantly with the increase of temperature. At room temperature of 25°C, the composite magnesium hydride hydrogen storage material is hydrolyzed in twice distilled water for 15 minutes to release hydrogen gas of 68.6% of the theoretical hydrogen storage cap...
Embodiment 3
[0021] The preparation method of the metal oxide composite magnesium hydride hydrogen storage material is as follows: using magnesium hydride as a base material, mixing metal oxide particles, the mass percentage of each component in the mixture is: magnesium hydride 97%, CeO 2 3%; the mixture is charged with hydrogen in a ball mill, and charged with hydrogen (0.4MPa) in a planetary ball mill for 100h, the ball-to-material ratio is 20:1, and the ball milling speed is 180r / min, and the obtained metal oxide is compositely hydrogenated The particle size of the magnesium hydrogen storage material is 28.0-60.0nm.
[0022] The hydrolysis rate of the obtained composite magnesium hydride hydrogen storage material increases significantly with the increase of temperature. At room temperature of 25°C, the composite magnesium hydride hydrogen storage material is hydrolyzed in seawater for 15 minutes to release hydrogen gas of 63.3% of the theoretical hydrogen storage capacity. At 50°C , t...
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