Preparation method of green degradable rice husk fast food oil absorption film
A rice husk and film technology, which is applied in the field of fast food film materials and rice husk fast food oil-absorbing films, can solve the problems of high cost and poor practicability, and achieve the effects of oil absorption capacity, easy cleaning and easy biodegradation
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Embodiment 1
[0025] Embodiment 1 A kind of preparation method of green degradable rice husk fast food oil-absorbing film comprises the steps:
[0026] (1) At room temperature, wash the rice husks with clean water, and then soak them in acetic acid solution overnight. The concentration of acetic acid solution is about 40wt%, then take them out, and dry them at a temperature of about 45°C, and then put them into steam In the explosion tank, and pass 0.8MPa water vapor into the steam explosion tank, keep it for 2 minutes, then open the steam explosion tank to quickly release the pressure, then wash with water and dry at 45°C;
[0027] (2) Dissolve chitosan and D,L-polylactic acid with a mass ratio of 1:5 in ethyl acetate to form a polymer solution, wherein the concentration of polylactic acid is about 20wt%, and the weight-average molecular weight of polylactic acid It is 120,000-140,000, and the weight average molecular weight of chitosan is 3-4 thousand;
[0028] Dissolve isopropyl triisos...
Embodiment 2
[0039] Embodiment 2 A kind of preparation method of green degradable rice husk fast food oil-absorbing film comprises the steps:
[0040] (1) After washing the rice husk with clear water, put it into the acetic acid solution for soaking, the temperature is 10°C, the time is 12h, the concentration of the acetic acid solution is 40wt%, then take it out, and bake it in an environment with a temperature of 40°C After drying, put it into a steam explosion tank, and pass 0.9MPa water vapor into the steam explosion tank, keep it for 3 minutes, then open the steam explosion tank to quickly release the pressure, then wash with water, and dry at 40°C;
[0041](2) Dissolve chitosan and D,L-polylactic acid with a mass ratio of 1:8 in ethyl acetate to form a polymer solution with a polylactic acid concentration of 10 wt%, wherein the polylactic acid has a weight-average molecular weight of 16- 180,000, the weight average molecular weight of chitosan is 5-6 thousand;
[0042] Dissolve isop...
Embodiment 3
[0047] Embodiment 3 A kind of preparation method of green degradable rice husk fast food oil-absorbing film comprises the steps:
[0048] (1) After washing the rice husks with clear water, put them into the acetic acid solution for soaking, the temperature is 25°C, the time is 2h, the concentration of the acetic acid solution is 32wt%, then take them out, and bake them in an environment with a temperature of 60°C After drying, put it into a steam explosion tank, and pass 1.0MPa water vapor into the steam explosion tank, keep it for 2 minutes, then open the steam explosion tank to quickly release the pressure, then wash with water, and dry at 60 °C;
[0049] (2) Dissolve chitosan and D,L-polylactic acid in ethyl acetate with a mass ratio of 1:10 to form a polymer solution with a polylactic acid concentration of 25 wt%, wherein the polylactic acid has a weight-average molecular weight of 15- 160,000, the weight average molecular weight of chitosan is 7-8 thousand;
[0050] Diss...
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