Method for vertical heteroepitaxy of single crystal metal film on the basis of single crystal copper
A metal thin film and heteroepitaxy technology, which is applied in the direction of single crystal growth, single crystal growth, chemical instruments and methods, etc., can solve the problems of single crystal substrates such as high price, application restrictions, small size, etc., to promote industrial production, The effect of low substrate cost and large size
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[0032] The invention provides a method for vertical heteroepitaxial single crystal metal thin film based on single crystal copper, the method comprises the following steps:
[0033] S1, using a chemical vapor deposition system to anneal commercial polycrystalline copper foil to convert it into single crystal copper foil, the annealing process is carried out according to the annealing process in the Chinese patent application CN201710020397.4; specifically, step S1 may include the following steps:
[0034] S11, forming one end of the polycrystalline copper foil so that the tip is flat on the high-temperature-resistant substrate, connecting the transmission device, putting it into the chemical vapor deposition equipment, passing in an inert gas with a flow rate of 300-500 sccm, and then starting to heat up , the heating process lasts for 50-70min, and the inert gas is N 2 or Ar;
[0035] S12, when the temperature rises to 800-1100°C, the polycrystalline copper foil gradually pa...
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