A kind of preparation method of dendrobium instant freeze-dried block
A dendrobium and freeze-drying technology, which is applied in the direction of freeze-drying transportation, medical preparations with non-active ingredients, medical preparations containing active ingredients, etc., can solve the problems of less dissolution of active ingredients, inconvenient taking, and influence on taking, and achieve Broad market application prospects, fast reconstitution speed, excellent reconstitution and instant effect
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Embodiment 1
[0030] (1) Remove the leaves from the fresh Dendrobium raw materials, and cut into small sections of 1-2 cm after cleaning;
[0031] (2) above-mentioned small section is placed in wall breaking device, mixes with the distilled water of 10 times of volumes, breaks wall 1min with the rotating speed of 30000rpm;
[0032] (3) the material of step (2) gained adopts three-legged centrifugal filtration, and its rotating speed is 500~800rpm;
[0033] (4) the solid obtained in step (3) is placed in a high-speed dispersing device, and is dispersed 3min with a rotating speed of 8000rpm;
[0034] (5) the material obtained in step (4) is placed in a high-pressure homogenization device to perform high-pressure homogenization twice, and each high-pressure homogenization includes a first homogenization and a second homogenization in turn, wherein the pressure of the first homogenization is 400Bar, and the pressure of the second homogenization is 1500Bar;
[0035] (6) in the material of step...
Embodiment 2
[0042] (1) Remove the leaves from the fresh Dendrobium raw materials, and cut into small sections of 1-2 cm after cleaning;
[0043](2) above-mentioned small section is placed in wall breaking device, mixes with the distilled water of 10 times of volumes, breaks wall 1min with the rotating speed of 30000rpm;
[0044] (3) the material of step (2) gained adopts three-legged centrifugal filtration, and its rotating speed is 500~800rpm;
[0045] (4) the solid obtained in step (3) is placed in a high-speed dispersing device, and is dispersed 3min with a rotating speed of 8000rpm;
[0046] (5) the material obtained in step (4) is placed in a high-pressure homogenization device to perform high-pressure homogenization twice, and each high-pressure homogenization includes a first homogenization and a second homogenization in turn, wherein the pressure of the first homogenization is 400Bar, and the pressure of the second homogenization is 1500Bar;
[0047] (6) in the material of step ...
Embodiment 3
[0054] (1) Remove the leaves from the fresh Dendrobium raw materials, and cut into small sections of 1-2 cm after cleaning;
[0055] (2) above-mentioned small section is placed in wall breaking device, mixes with the distilled water of 10 times of volumes, breaks wall 1min with the rotating speed of 30000rpm;
[0056] (3) the material of step (2) gained adopts three-legged centrifugal filtration, and its rotating speed is 500~800rpm;
[0057] (4) the solid obtained in step (3) is placed in a high-speed dispersing device, and is dispersed 3min with a rotating speed of 8000rpm;
[0058] (5) the material obtained in step (4) is placed in a high-pressure homogenization device to perform high-pressure homogenization twice, and each high-pressure homogenization includes a first homogenization and a second homogenization in turn, wherein the pressure of the first homogenization is 400Bar, and the pressure of the second homogenization is 1500Bar;
[0059] (6) in the material of step...
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