Preparation method for controllable degradation type zinc-magnesium gradient material
A gradient material, zinc-magnesium technology, applied in the preparation and application of medical biomaterials, can solve the problem that it is difficult to meet the diversity of degradable implant materials
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[0070] The present invention will be further described below in conjunction with accompanying drawing:
[0071] figure 1 As shown in ., it is the state diagram of spark plasma sintering of magnesium-zinc gradient mixed powder. It is necessary to connect all parts correctly and operate in sequence.
[0072] Quantities of chemicals used in preparation determined in pre-set ranges in grams, milliliters, microns, moles / liter, centimeters 3 is the unit of measurement.
[0073] The sintering of the magnesium-zinc gradient mixed powder is carried out in the spark plasma sintering furnace protected by argon gas, and is completed during the heating process of the discharge plasma;
[0074] The discharge plasma sintering furnace is vertical, including a vacuum sintering furnace 1, the lower part of the vacuum sintering furnace 1 is a base 3, the upper part is a top seat 2, and the interior is a furnace cavity 39; Vacuum pump 6, water tank 8; Vacuum tube 7 is provided on the top of va...
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