Novel hindered amine light stabilizer preparation method
A hindered amine light stabilizer, a new type of technology, applied in the direction of rayon manufacturing, single-component polyolefin rayon, fiber chemical characteristics, etc., can solve the problem of heavy taste, achieve good compatibility, processing performance and anti-corrosion Excellent aging effect and fewer steps for product synthesis
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0028] Add 300g of toluene as a solvent, 76.08g of vanillin, 45.22g of sodium chlorite in a 1000ml four-neck bottle assembled with a condenser, a water separator, a foam blower, a return pipe, a thermometer and an agitator, and open Stir and react at 120°C for 2h. After cooling down to 30°C, add 32.04g of methanol, start stirring, react at 100°C for 2 hours, add 78.63g of tetramethylpiperidinol, raise the temperature to 140°C and continue stirring for 3 hours, then wash with water, decolorize, filter, cool and crystallize to obtain the target Product 136.3g.
[0029] Product evaluation experiment:
[0030] Maximum breaking force before aging (N) Maximum breaking force after aging (N) Fracture Maximum Force Retention % 3‰783 69 43 62.3 3‰ target product 72 51 70.8
Embodiment 2
[0032] Add 400g of toluene as solvent, 152.15g of vanillin, 90.44g of sodium chlorite in a 1000ml four-necked bottle assembled with condenser, water separator, foamer, return pipe, thermometer and stirrer, and open Stir and react at 100°C for 1h. After cooling down to 30°C, add 64.08g of methanol, start stirring, react at 80°C for 1 hour, add 157.25g of tetramethylpiperidinol, raise the temperature to 120°C and continue stirring for 5 hours, then wash with water, decolorize, filter, and cool to crystallize to obtain the target Product 271.2g.
[0033] Product evaluation experiment:
[0034] Maximum breaking force before aging (N) Maximum breaking force after aging (N) Fracture Maximum Force Retention % 3‰783 71 45 63.4 3‰ target product 73 54 73.9
Embodiment 3
[0036] Add 800g of toluene as solvent, 304.3g of vanillin, 180.88g of sodium chlorite in a 2000ml four-necked bottle assembled with condenser, water separator, foamer, return pipe, thermometer and stirrer, and open Stir and react at 60°C for 0.5h. After cooling down to 30°C, add 128.16g of methanol, start stirring, react at 60°C for 0.5h, add 314.5g of tetramethylpiperidinol, raise the temperature to 100°C and continue stirring for 1h, then wash with water, decolorize, filter, and cool to crystallize to obtain Target product 518.9g.
[0037] Product evaluation experiment:
[0038] Maximum breaking force before aging (N) Maximum breaking force after aging (N) Fracture Maximum Force Retention % 3‰783 69 43 62.3 3‰ target product 73 51 69.9
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com