3,4-methylenedioxy methcathinone detection methods
A dioxymethcathinone and methylene technology, which is applied in the detection field of 3,4-methylenedioxymethcathinone, can solve the problems of lack of new psychoactive substances and the like
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Embodiment 1
[0097] Embodiment 1, carry out qualitative analysis to Methylone in suspected drug sample with gas chromatography-mass spectrometry (GC-MS)
[0098] 1. Reagents and standard substances, instruments and measuring instruments
[0099] 1.1 Reagents and standard substances
[0100] All reagents used in this method are of analytical grade.
[0101] Extraction reagent: Methanol.
[0102] Traceable reference material: Methylone.
[0103] 1.2 Instruments and measuring instruments
[0104] Gas Chromatograph (GC) equipped with Flame Ionization Detector (FID).
[0105] Gas chromatography-mass spectrometry (GC-MS), a quadrupole mass spectrometer equipped with a standard electron impact (EI) source.
[0106] centrifuge.
[0107] Electronic balance, actual division value d=0.01mg.
[0108] oscillator.
[0109] 10mL and 1mL pipettes or pipettes.
[0110] 10mL bottle top pipette.
[0111] Note: All instruments and measuring instruments involved must pass the metrological verificatio...
Embodiment 2
[0136] Embodiment 2, gas chromatography-hydrogen flame ionization detector (GC-FID) carries out quantitative analysis to the Methylone in the suspected drug sample
[0137] 1. Reagents and standard substances, instruments and measuring instruments
[0138] 1.1 Reagents and standard substances
[0139] All reagents used in this method are of analytical grade.
[0140] Extraction reagent: Methanol.
[0141] Traceable reference material: Methylone.
[0142] 1.2 Instruments and measuring instruments
[0143] Gas Chromatograph (GC) equipped with Flame Ionization Detector (FID).
[0144] Gas chromatography-mass spectrometry (GC-MS), a quadrupole mass spectrometer equipped with a standard electron impact (EI) source.
[0145] centrifuge.
[0146] Electronic balance, actual division value d=0.01mg.
[0147] oscillator.
[0148] 10mL and 1mL pipettes or pipettes.
[0149] 10mL bottle top pipette.
[0150] Note: All instruments and measuring instruments involved must pass the ...
Embodiment 3
[0232] Example 3, Methylone in suspected drug samples was qualitatively analyzed by liquid chromatography-tandem mass spectrometry (LC-MS / MS) in multiple reaction monitoring (MRM) mode
[0233] 1. Reagents and standard substances, instruments and measuring instruments
[0234] 1.1 Reagents and standard substances
[0235] The reagents used are chromatographically pure, and the test water is first-grade water (see GB / T 6682-2008). The reagents and standard substances include:
[0236] a) Reagents: methanol, acetonitrile, formic acid;
[0237] b) Traceable reference material: Methylone;
[0238] c) 0.1% formic acid aqueous solution: measure 1mL of formic acid, add water to dissolve and dilute to 1000mL, mix well, filter through a 0.22μm filter membrane, and let it stand for use after ultrasonication;
[0239] d) Standard stock solution: Weigh the Methylone standard substance, dissolve it with methanol respectively, prepare the standard stock solution of 2.5 mg / mL, store it in...
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