A kind of two-component interface agent and preparation method thereof
An interface agent, two-component technology, used in coatings, anti-corrosion coatings, etc., can solve the problems of aging resistance, slow drying speed, poor water resistance, etc. Effect
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Embodiment 1
[0070] Component A synthesis raw materials: 20 parts of n-butyl acrylate, 12 parts of methyl methacrylate, 8 parts of styrene, 2 parts of vinyl tertiary carbonate (Veova 9), 5 parts of glycidyl methacrylate, 2 parts of acrylic acid, 0.4 parts of initiator, 1.125 parts of compound emulsifier, 60 parts of water.
[0071] Synthetic raw materials for component B: 5 parts of 3-aminopropyltriethoxysilane, 10 parts of ethanol, 85 parts of water, and 1 part of glacial acetic acid as a pH regulator.
[0072] Its preparation steps are:
[0073] Component A: 20 parts of n-butyl acrylate, 12 parts of methyl methacrylate, 8 parts of styrene, 2 parts of vinyl tertiary carbonate (Veova 9), 5 parts of glycidyl methacrylate, 2 parts of acrylic acid, compound Add 1 part of emulsifier (0.8 part of SE-10N, 0.2 part of SDS) and 30 parts of water into a four-necked flask, stir for 30 minutes, and rotate at a speed of about 500 rad / min to obtain a milky white uniform pre-emulsion, and then 1 / 3 of t...
Embodiment 2
[0077] Synthetic raw materials for component A: 16 parts of n-butyl acrylate, 8 parts of methyl methacrylate, 12 parts of styrene, 5 parts of vinyl tertiary carbonate (Veova 9), 5 parts of glycidyl methacrylate, 3 parts of acrylic acid, 0.5 parts of initiator, 1.2 parts of composite emulsifier, 80 parts of water, 2 parts of pH regulator 2-amino-2-methyl-1-propanol, 0.2 parts of bronopol fungicide;
[0078] Synthetic raw materials for component B: 10 parts of 3-aminopropyltriethoxysilane, 15 parts of ethanol, 75 parts of water, 2 parts of acrylic acid as a pH regulator, and 0.1 part of bronopol fungicide;
[0079] Its preparation steps are:
[0080] Component A: 16 parts of n-butyl acrylate, 8 parts of methyl methacrylate, 12 parts of styrene, 5 parts of vinyl tertiary carbonate (Veova 9), 5 parts of glycidyl methacrylate, 3 parts of acrylic acid, compound Add 1.05 parts of emulsifier (0.9 parts of SR10, 0.15 parts of SDS) and 50 parts of water into a four-necked flask, stir f...
Embodiment 3
[0084] Synthetic raw materials for component A: 32 parts of n-butyl acrylate, 15 parts of methyl methacrylate, 15 parts of styrene, 4 parts of vinyl tertiary carbonate (Veova 10), 4 parts of glycidyl methacrylate, 2 parts of acrylic acid, 0.5 parts of initiator, 1.2 parts of compound emulsifier, 100 parts of water, 1 part of pH regulator N,N-dimethylethanolamine, 0.2 parts of bronopol fungicide;
[0085] Synthetic raw materials for component B: 5 parts of γ-ureidopropyltriethoxysilane, 20 parts of ethanol, 75 parts of water, 1 part of acrylic acid with pH regulator, 0.1 part of bronopol fungicide;
[0086] Its preparation steps are:
[0087]Component A: 32 parts of n-butyl acrylate, 15 parts of methyl methacrylate, 15 parts of styrene, 4 parts of vinyl tertiary carbonate (Veova 10), 4 parts of glycidyl methacrylate, 2 parts of acrylic acid, compound Add 1.05 parts of emulsifier (0.9 part of COPS-1, 0.15 part of SDS) and 60 parts of water into a four-neck flask, stir for 30 mi...
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