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Manufacturing device and method for high-tenacity nano-particle-reinforced aluminum matrix composite material

A nanoparticle and composite device technology, applied in chemical instruments and methods, mixers with rotary stirring devices, mixers, etc., can solve the problems of low strength and toughness of composite materials, limited strength improvement, limited processing area, etc. Strength and toughness, improve severe agglomeration, strong continuity

Active Publication Date: 2019-08-20
JIANGSU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are still two major problems with the in-situ-generated nanoparticle-reinforced Al-matrix composites: (1) Due to the huge interfacial energy of the nanoparticles, the in-situ-generated nanoparticles tend to agglomerate, resulting in low strength and toughness of the composite; (2) Generally, the grains of cast aluminum matrix composites are coarse, and the strength improvement is limited
However, the existing technology is difficult to achieve large-scale continuous production. For example, the invention patent of the domestic publication No. CN103668013B "A method for superplastic pretreatment of in-situ aluminum-based composite materials", the in-situ nanoparticle-reinforced aluminum-based composite materials obtained in the as-cast state are processed. Friction stir processing (FSP) treatment makes the distribution of nanoparticles uniform, and obtains ultra-fine-grained aluminum-based composites, which can improve the strength and plasticity at the same time. However, the FSP process is complex and the processing area is extremely limited, making it difficult to realize industrial applications.

Method used

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  • Manufacturing device and method for high-tenacity nano-particle-reinforced aluminum matrix composite material
  • Manufacturing device and method for high-tenacity nano-particle-reinforced aluminum matrix composite material
  • Manufacturing device and method for high-tenacity nano-particle-reinforced aluminum matrix composite material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] with K 2 ZrF 6 and KBF 4 As a reactant, according to generate 3vol% nano ZrB 2The particles are chemically proportioned, and the mixed and ground reactant powder is dried at 200°C for 2 hours for later use; the 6016 aluminum alloy is placed in a spiral circulation stirring composite device, and is heated and melted by an induction coil. When the temperature reaches 870°C, the Add the mixed and ground reactant powder to the spiral circulation stirring compound device; turn on the spiral circulation stirring compound device, the speed is 10-30r / min and react for 30 minutes, increase the speed of the spiral circulation stirring compound device to 30-50r / min, and stir for 20 minutes After that, let it stand still, degas and remove slag, and pass it into the screw extrusion device when the temperature drops to 720°C. Then continue to cool down to 300°C, turn on the screw extrusion device at a speed of 20-50r / min, extrude the aluminum-based composite material to the mold, ...

Embodiment 2

[0032] with K 2 ZrF 6 and Na 2 B 4 o 7 As a reactant, according to generate 5vol% nano ZrB 2 +Al 2 o 3 The particles are chemically proportioned, and the mixed and ground reactant powder is dried at 300°C for 3 hours for later use; the 6082 aluminum alloy is placed in a spiral circulation stirring composite device, and is heated and melted by an induction coil. When the temperature reaches 850°C, the Mix and grind the reactant powder into the spiral circulation stirring compound device; turn on the spiral circulation stirring compound device, the speed is 10-30r / min, after reacting for 30 minutes, increase the speed of the spiral circulation stirring compound device to 30-50r / min, stir After 20 minutes, let it stand still, degas and remove slag, and pass it into the screw extrusion device when the temperature drops to 720°C. Afterwards, continue to cool down to 400°C, turn on the screw extrusion device at a speed of 50-80r / min, and extrude the aluminum-based composite m...

Embodiment 3

[0034] with K 2 ZrF 6 , K 2 TiF 6 and KBF 4 As a reactant, according to generate 3vol% ZrB 2 Granules, 1vol% TiB 2 Carry out stoichiometric proportioning of the particles, and dry the mixed and ground reactant powder at 200°C for 3 hours for later use; place 7055Al in a spiral circulation stirring composite device, heat and melt with an induction coil, and when the temperature reaches 900°C, mix and grind The final reactant powder is added to the spiral circulation stirring compound device; turn on the spiral circulation stirring compound device, the speed is 10-30r / min, after 30 minutes of reaction, increase the speed of the spiral circulation stirring compound device to 30-50r / min, after stirring for 20 minutes , standing still, degassing, and slag removal, and when the temperature drops to 720 ° C, it is passed into the screw extrusion device. Afterwards, continue to cool down to 450°C, turn on the screw extrusion device at a speed of 70-100r / min, and extrude the alum...

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Abstract

The invention relates to an aluminum matrix composite material, in particular to a manufacturing device and method for a high-tenacity nano-particle-reinforced aluminum matrix composite material. Themanufacturing device and method is characterized in that based on a designed spiral circulation stirring combination and compression integrated device, firstly an aluminum alloy matrix is placed in aspiral circulation stirring combination device and is heated to certain temperature and molten; an in-situ reactant; in-situ nano-combination is realized by virtue of the effect of spiral circulationstirring; then an in-situ combination melt is directly introduced into a spiral compression device, and is cooled to lower temperature in the spiral compression device; nano-particle cluster breakingand matrix crystal grain refining in the in-situ combined nano-particle-reinforced aluminum matrix combination material are realized by utilizing a large deformation shearing effect which is generatedby movement of a lead screw in the spiral compression device; and finally the material is formed through an extrusion end mould to obtain the high-tenacity nano-particle-reinforced aluminum matrix composite material of a required shape.

Description

technical field [0001] The invention relates to an aluminum-based composite material, in particular to a preparation device and method for a high-strength nano particle-reinforced aluminum-based composite material. Background technique [0002] The in-situ synthesis process of aluminum-based composites is a new technology developed in recent years. In-situ endogenous particle-reinforced aluminum-based composites have the advantages of small reinforcement size, good thermal stability, and high interface bonding strength. They are used in aviation, aerospace, It has a wide range of applications in industrial fields such as automobiles and machinery. Some studies in recent years have shown that when the particle size of the reinforcement is reduced to the nanometer level, the surface area of ​​the nanoparticles per unit volume increases sharply, and the composite strengthening effect is greatly improved, so that the nanoparticle-reinforced aluminum matrix composite has a higher...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C1/10C22C1/02C22C21/00C22C32/00B01F13/10B01F7/24
CPCC22C1/1036C22C21/00C22C32/0005C22C32/0036C22C32/0073B01F27/92B01F33/811C22C1/1047
Inventor 怯喜周武林黄烁铭彭艳杰陈刚赵玉涛
Owner JIANGSU UNIV
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