Polycarboxylate dispersing agent and preparation method thereof
A polycarboxylate and dispersant technology, applied in the field of pesticides, can solve the problems of poor environmental compatibility, low molecular weight, unreasonable distribution of functional groups, etc., and achieve the effects of high dispersion performance and stability performance, and uniform structure distribution.
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Embodiment 1
[0024] Step 1: Take the following quality materials: 30 parts of itaconic acid, 200 parts of deionized water and 1 part of mercaptoacetic acid are added to a four-neck flask with a stirrer, constant pressure dropping funnel, thermometer, and condenser, and the temperature is raised with stirring Keep warm at about 80°C for 2 hours;
[0025] Step 2: Add 30 parts of monomer allyl polyoxyethylene ether and 5 parts of initiator ammonium persulfate dropwise to the above solution within 2.5 hours, and keep warm for 4 hours;
[0026] Step 3: Finally, 6 parts of pH regulator NaOH were added to the above solution, stirred for neutralization, cooled and discharged to obtain a polycarboxylate dispersant.
Embodiment 2
[0028] Step 1: Take the following quality materials: 30 parts of acrylic acid, 200 parts of deionized water and 1 part of mercaptoacetic acid are added to a four-necked flask with a stirrer, a constant pressure dropping funnel, a thermometer and a condenser, and the temperature is raised to 80 Keep warm at about ℃ for 2 hours;
[0029] Step 2: Add 30 parts of monomer methallyl polyoxyethylene ether and 5 parts of initiator ammonium persulfate to the above solution dropwise within 2.5 hours, and keep warm for 4 hours;
[0030] Step 3: Finally, 6 parts of pH regulator NaOH were added to the above solution, stirred for neutralization, cooled and discharged to obtain a polycarboxylate dispersant.
Embodiment 3
[0032] Step 1: Take the following quality materials: 30 parts of methacrylic acid, 200 parts of deionized water and 1 part of mercaptoacetic acid are added to a four-necked flask with a stirrer, a constant pressure dropping funnel, a thermometer and a condenser tube, and the temperature is raised with stirring Keep warm at about 80°C for 2 hours;
[0033] Step 2: Add 30 parts of monomer nonylphenol polyoxyethylene ether acrylate and 5 parts of initiator ammonium persulfate to the above solution dropwise within 2.5 hours, and keep warm for 4 hours;
[0034] Step 3: Finally, 6 parts of pH regulator NaOH were added to the above solution, stirred for neutralization, cooled and discharged to obtain a polycarboxylate dispersant.
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