A method for preparing triphenyl phosphate by extracting phenol from aryl phosphate production wastewater
A technology of triphenyl phosphate and aryl phosphate, which is applied in the field of extracting phenol from aryl phosphate production wastewater to prepare triphenyl phosphate, can solve the problems of increasing wastewater treatment capacity, only downgrading use, poor quality of finished products, etc.
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Embodiment 1
[0043] 1) Add 80.8kg of pickling wastewater to 300kg of alkali washing wastewater, stir at 40-60°C for 1 hour, adjust the pH value to 6-7, and then let it stand for 1 hour to separate 23.3kg of the lower oil layer and 355.46 kg of the upper layer of wastewater kg; Measure the phenol content of the upper layer wastewater to 22188ppm (phenol content detection: liquid chromatography external standard method);
[0044] 2) Add 29.62 kg of triphenyl phosphate extractant to the upper layer of wastewater obtained in step 1), the amount of the extractant added is 1 / 12 of the quality of the upper layer of wastewater, stirred for 1 hour at a temperature of 50-60 ° C, and then allowed to stand for 1 hour , separate 347.3kg water layer (the phenol content 887ppm of described water layer) and 37.42kg extraction layer, record the extraction layer phenol content 20152ppm;
[0045] 3) Transfer the extraction layer obtained in step 2) into a distillation kettle for dehydration by distillation u...
Embodiment 2
[0054] Other steps of embodiment 2 are identical with embodiment 1, and difference is that in step 1) after adding acid waste water, adjust pH value in waste water to be 2, measure step 1) the phenol content of upper layer waste water is 20158ppm.
Embodiment 3
[0055] The other steps of embodiment 3 are the same as in embodiment 1, except that in step 2), the extraction agent addition ratio is 1 / 10 of the water layer quality, and the final measurement step 2) the phenol content of the water layer is 573ppm.
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