Corrosive agent and corrosion method for dendritic tissue of CoCrMo alloy used in artificial joint
A technology of dendritic structure and artificial joint is applied in the field of metallographic structure characterization of metal materials, which can solve the problem of inability to display dendritic structure, and achieve the effect of simple composition, good reproducibility and clear structure.
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Embodiment 1
[0029] 1. Specimen Preparation
[0030] Select a CoCrMo alloy artificial joint in the as-cast state, and cut a metallographic sample of Ф15*12mm. The sample is mechanically polished and polished according to the metallographic sample preparation method. The sample is first mechanically polished by 120#, 200#, 400#, 600#, 800#, 1000#, 1200# water-grinding sandpaper; Carry out mechanical polishing for 3.5μm and 1.5μm polishing paste, polish until the surface is free of scratches, rinse with water, then clean with alcohol and dry, pay attention to the corrosion surface without water stains.
[0031] 2. Corrosive preparation
[0032] First, use a measuring cylinder to measure 30ml of potassium permanganate solution with a concentration of 8%, and pour it into a beaker; then measure 30ml of a sodium hydroxide solution with a concentration of 20%, and pour it into a beaker with potassium permanganate solution. Stir with a glass rod to mix the solution thoroughly.
[0033] 3. Corr...
Embodiment 2
[0036] 1. Specimen Preparation
[0037] Select a CoCrMo alloy artificial joint in the heat treatment state, and cut a metallographic sample of Ф15*10mm. The sample is mechanically polished and polished according to the metallographic sample preparation method. The sample is first mechanically polished by 120#, 200#, 400#, 600#, 800#, 1000#, 1200# water-grinding sandpaper; Carry out mechanical polishing for 3.5μm and 1.5μm polishing paste, polish until the surface is free of scratches, rinse with water, then clean with alcohol and dry, pay attention to the corrosion surface without water stains.
[0038] 2. Corrosive preparation
[0039] First, use a measuring cylinder to measure 25ml of potassium permanganate solution with a concentration of 8%, and pour it into a beaker; then measure 25ml of a sodium hydroxide solution with a concentration of 20%, and pour it into a beaker with potassium permanganate solution. Mix the solution thoroughly with a glass rod.
[0040] 3. Corro...
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