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Production technology of Mucuna Pruriens extract products

A production process and extract technology, which is applied in the production process of quinoa bean extract, can solve the problems of increased environmental protection pressure, short service life of filter membrane, low extraction rate, etc., to ensure product sales, increase product yield, The effect of high product yield

Inactive Publication Date: 2019-02-01
那坡康正天然植物提取有限责任公司
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  • Abstract
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  • Application Information

AI Technical Summary

Problems solved by technology

The more prominent problem of the acid water-resin method is that the extraction process consumes a large amount of hydrochloric acid, which requires particularly high acid resistance of the equipment, resulting in short service life of the equipment, quick update, and high production costs; another obvious disadvantage of the acid water-resin method is : The production process produces a large amount of acidic wastewater, and after neutralization, a large amount of protein precipitates are precipitated. The COD is as high as 10,000 mg / L, which seriously exceeds the national discharge standard of COD less than 100 mg / L. Therefore, this type of sewage treatment facility requires large investment and environmental protection. The cost is extremely high, the pressure on environmental protection increases, and the product cost is high
The disadvantage is that after the particles and colloidal ions in the extract are adsorbed and deposited on the membrane surface or in the membrane pores to a certain extent, the membrane pores are quickly blocked and become smaller, and the permeation flow and separation characteristics of the membrane are irreversibly changed. Phenomenon, the membrane permeability and transmittance are almost 0, and the membrane needs to be regenerated frequently, so that the service life of the filter membrane is very short, and the filter membrane needs to be updated frequently, and the cost is very high
But this method has the following disadvantages: the pH adjusted by the extract is 5.5-8, and finally there will be about 5% of acid-base wastewater to be discharged, and more components such as ammonium bicarbonate, ammonium sulfate, and tannin are added in the extraction process Acid, sodium metabisulfite, etc., increase the cost and cause some pollution to the environment; cat beans are extracted after being flattened, and cannot obtain levodopa to a greater extent, and the product yield is only 3-3.5%, which needs to be improved
[0006] At present, the processing and production of levodopa by quinoa beans generally has defects such as complicated procedures, low extraction rate, low purity of levodopa, and high cost.
Due to the particularity of the extraction of lentil beans, the current production cost of levodopa from quinoa beans remains high and cannot compete with low-content levodopa that is chemically synthesized or blended with high-content levodopa and starch. The pharmacological effect of the extract is obviously better than blended dopa, but because of its extremely high price, it affects sales and cannot fully open up the market

Method used

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  • Production technology of Mucuna Pruriens extract products
  • Production technology of Mucuna Pruriens extract products

Examples

Experimental program
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Effect test

Embodiment 1

[0029] A kind of production technology of quinoa bean extract, comprises the steps:

[0030] (1) Treatment of quinoa beans: Clean the quinoa beans, grind them into powder, and pass through a 50-mesh sieve to obtain quinoa bean powder; vacuum-seal the quinoa bean powder, the thickness of the packed quinoa bean powder is 8mm, and transfer it to Zhongneng The irradiation treatment is carried out in the electron accelerator, the output energy of the electron beam is 1.5MeV, the output power is 80KW, and the transmission speed of the quinoa bean powder is 12m / min.

[0031] (2) Leaching: vitamin B3 and citric acid were added to dissolve in water, and sucrose ester was added simultaneously, and the addition amount of the sucrose ester was 0.05% of water weight; then, quinoa bean powder was added and mixed, ultrasonically extracted for 30min, ultrasonically The power is 900W, and the working temperature is 55°C; then reflux extraction for 18 hours, filter, the extraction solution is f...

Embodiment 2

[0037] A kind of production technology of quinoa bean extract, comprises the steps:

[0038](1) Treatment of quinoa beans: Clean the quinoa beans, grind them into powder, and pass through a 50-mesh sieve to obtain quinoa bean powder; vacuum-seal the quinoa bean powder, the thickness of the packed quinoa bean powder is 6mm, and transfer it to Zhongneng The irradiation treatment is carried out in the electron accelerator, the output energy of the electron beam is 1.0MeV, the output power is 60KW, and the transmission speed of the quinoa bean powder is 11m / min.

[0039] (2) Leaching: vitamin B3 and citric acid were added to dissolve in water, and sucrose ester was added simultaneously, and the addition of said sucrose ester was 0.04% of water weight; then, quinoa bean powder was added and mixed, ultrasonically extracted for 40min, ultrasonically The power is 850W, and the working temperature is 55°C; then reflux extraction for 16 hours, filter, and the extract is used for standby...

Embodiment 3

[0045] A kind of production technology of quinoa bean extract, comprises the steps:

[0046] (1) Treatment of quinoa beans: Clean the quinoa beans, grind them into powder, and pass through a 50-mesh sieve to obtain quinoa bean powder; vacuum-seal the quinoa bean powder, the thickness of the packed quinoa bean powder is 8mm, and transfer it to Zhongneng The irradiation treatment is carried out in the electron accelerator, the output energy of the electron beam is 2.0MeV, the output power is 90KW, and the transmission speed of the quinoa bean powder is 14m / min.

[0047] (2) Leaching: vitamin B3 and citric acid were added to dissolve in water, and sucrose ester was added simultaneously, and the addition amount of the sucrose ester was 0.07% of water weight; then, quinoa bean powder was added and mixed, ultrasonically extracted for 25min, ultrasonically The power is 950W, and the working temperature is 55°C; then reflux extraction for 19 hours, filter, and the extract is used for ...

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Abstract

The invention discloses a production technology of Mucuna Pruriens extract products, and belongs to the technical field of advanced processing of Mucuna Pruriens. The technology comprises the following steps: processing Mucuna Pruriens to obtain Mucuna Pruriens powder; adding vitamin B3 and citric acid into water to achieve dissolving, adding the Mucuna Pruriens powder, performing uniform mixing,carrying out ultrasonic extraction, then carrying out refluxing extraction, adjusting the pH value of the obtained solution to 4.5-5.5, standing the obtained solution for precipitation to obtain an extract liquid, centrifuging the extract liquid, and drying the obtained precipitate and mother liquor to obtain Mucuna Pruriens extract I; and concentrating the above obtained supernatant to obtain a crude product, and refining, drying, crushing, mixing and packaging the crude product to obtain Mucuna Pruriens extract II. The technology has the advantages of less flow, no pollutant emission, high yield and high purity of the Mucuna Pruriens extract products, small consumption of an extractant, and easiness in industrial production. The cost of the technology is far lower than that of traditional technologies, and is close to the blending cost of low-content dihydroxyphenylalanine. A series of products containing 10-99% of the Mucuna Pruriens extract products can be produced through the technology, so the technology can meet demands of different clients, and ensures the sales quality of the products.

Description

technical field [0001] The invention belongs to the technical field of quinoa bean deep processing, and in particular relates to a production process of a quinoa bean extract. Background technique [0002] Quinoa bean is the dry seed of the plant of the genus Quinoa chinensis. It is mainly produced in Guangxi, Guizhou and other regions of my country. At present, quinoa bean is widely used in medicine to treat Parkinson's disease, poisonous snake bites, male infertility and other diseases. Levodopa is the main active ingredient. Levodopa is one of the precursors for the synthesis of norepinephrine and dopamine in the body, which can increase the level of dopamine in the brain tissue. It is an important biologically active substance in the body. important intermediates in biochemical metabolic pathways. At present, levodopa products are made by blending high-content levodopa and starch in a certain proportion (so called blended dopa). Although the cost is low, its pharmacolog...

Claims

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Application Information

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IPC IPC(8): C07C229/36C07C227/40
CPCC07C227/40C07C229/36
Inventor 陆华黎永红黎敏护
Owner 那坡康正天然植物提取有限责任公司
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