Preparation method of rock salt type (MgCoCuNiZn)O high entropy oxide powder material
An oxide powder, rock salt type technology, applied in chemical instruments and methods, cobalt compounds, inorganic chemistry, etc., can solve the problems of high energy consumption and complex preparation process, achieve uniform distribution, simple and easy process, and high production efficiency Effect
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Embodiment 1
[0021] Weigh 12.82g of Mg(NO 3 ) 2 .6H 2 O, 14.55g of Co(NO 3 ) 2 .6H 2 O, 12.08g of Cu(NO 3 ) 2 .3H 2 O, 14.54g of Ni(NO 3 ) 2 .6H 2 O and 14.87g of Zn(NO 3 ) 2 .6H 2 O was dissolved in 62.5mL of distilled water and stirred evenly to obtain a mixed solution containing metal salts; then 75.05g of tartaric acid and 2.25g of ammonium nitrate were weighed and added to the above mixed solution, after stirring evenly, the pH of the mixed solution was adjusted to 7 with ammonia water to obtain a transparent Then heat the above transparent sol in an oil bath at 150°C to remove the solvent water to obtain a loose, foamy gel; finally place the above gel in a muffle furnace at 300°C for 30 minutes to obtain a rock salt type Crystal structure (such as figure 1 shown), the spherical rock-salt structure (MgCoCuNiZn)O high-entropy oxide nanopowder material with an average particle size of 25 nm (such as figure 2 shown).
Embodiment 2
[0023] Weigh 12.82g of Mg(NO 3 ) 2 .6H 2 O, 14.55g of Co(NO 3 ) 2 .6H 2 O, 12.08g of Cu(NO 3 ) 2 .3H 2 O, 14.54g of Ni(NO 3 ) 2 .6H 2 O and 14.87g of Zn(NO 3 ) 2 .6H 2 O was dissolved in a solvent composed of 42.5mL distilled water and 7.5mL ethanol, and stirred evenly to obtain a mixed solution containing metal salts; then 86.45g of citric acid was weighed and added to the above mixed solution, and after stirring evenly, the pH of the mixed solution was adjusted to 6 with ammonia water , to obtain a transparent sol; then heat the above transparent sol in a water bath at 80°C to remove the solvent water, and obtain a loose, foamy gel; finally place the above gel in a muffle furnace at 550°C for 15 minutes to obtain The spherical rock-salt structure (MgCoCuNiZn)O high-entropy oxide nanopowder material with an average particle size of 80nm.
Embodiment 3
[0025] Weigh 12.82g of Mg(NO 3 ) 2 .6H 2 O, 14.55g of Co(NO 3 ) 2 .6H 2 O, 12.08g of Cu(NO 3 ) 2 .3H 2 O, 14.54g of Ni(NO3 ) 2 .6H 2 O and 14.87g of Zn(NO 3 ) 2 .6H 2 O was dissolved in 33.3mL of distilled water, stirred evenly to obtain a mixed solution containing metal salts; then weighed 43.22g of citric acid, 72.06g of glucose and 1.2g of ammonium acetate into the above mixed solution, stirred evenly and adjusted the pH of the mixed solution with ammonia water 8, a transparent sol was obtained; then the above transparent sol was heated in an oil bath at 200°C to remove the solvent water, and a loose, foamy gel was obtained; finally, the above gel was placed in a microwave oven with a power of 600W to react After 5 minutes, a spherical rock-salt structure (MgCoCuNiZn)O high-entropy oxide nanopowder material with an average particle size of 120 nm was obtained.
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