Seawater desalinizing scale inhibitor and preparation method thereof
A scale inhibitor and water-soluble technology, applied in the field of seawater desalination scale inhibitor and its preparation, can solve the problems of poor scale inhibitor dispersion, poor corrosion inhibition performance, insufficient environmental protection, etc., and achieves good temperature resistance, low cost and effect. long lasting effect
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Embodiment 1
[0024] Weigh 1 part of trisodium phosphate according to the ratio of parts by weight; 2 parts of amino trimethylene phosphonic acid; 2 parts of polyaspartic acid; 3 parts of benzotriazole; 100 parts of water; 4 parts of chitosan; boric acid 5 parts of zinc; 2.5 parts of water-soluble copper sulfide; 6 parts of gluconic acid; 1 part of sodium hypophosphite; 1 part of phosphonic acid; 0.5 part of 2-mercaptobenzothiazole.
[0025] Add gluconic acid and water into a four-neck flask equipped with an electric stirrer, a constant pressure dropping funnel, a thermometer and a reflux condenser, heat to 60°C, stir for 5 minutes, add trisodium phosphate and benzotriazole dropwise, and heat up To 80°C, react for 2h.
[0026] Add ethylenediamine, water-soluble copper sulfide, polyaspartic acid and sodium hypophosphite, raise the temperature to 100°C, and react for 1h.
[0027] Raise the temperature to 120°C, add the remaining raw materials, stir for 50 minutes, cool to room temperature a...
Embodiment 2
[0030] Take by weight 5 parts of trisodium phosphate; 8 parts of amino trimethylene phosphonic acid; 6 parts of polyaspartic acid; 7 parts of benzotriazole; 100 parts of water; 6 parts of chitosan; boric acid 9 parts of zinc; 6.5 parts of water-soluble copper sulfide; 10 parts of gluconic acid; 9 parts of sodium hypophosphite; 3 parts of phosphonic acid; 4.5 parts of 2-mercaptobenzothiazole.
[0031] Add gluconic acid and water into a four-neck flask equipped with an electric stirrer, a constant pressure dropping funnel, a thermometer and a reflux condenser, heat to 80°C, stir for 25 minutes, add trisodium phosphate and benzotriazole dropwise, and heat up To 100°C, react for 4h.
[0032] Add ethylenediamine, water-soluble copper sulfide, polyaspartic acid and sodium hypophosphite, raise the temperature to 120°C, and react for 6h.
[0033] Raise the temperature to 140°C, add the remaining raw materials, stir for 90 minutes, cool to room temperature and discharge to obtain the...
Embodiment 3
[0036] Take by weight 3 parts of trisodium phosphate; 5 parts of amino trimethylene phosphonic acid; 4 parts of polyaspartic acid; 5 parts of benzotriazole; 100 parts of water; 5 parts of chitosan; boric acid 7 parts of zinc; 4.5 parts of water-soluble copper sulfide; 8 parts of gluconic acid; 8 parts of sodium hypophosphite; 2 parts of phosphonic acid; 2.5 parts of 2-mercaptobenzothiazole.
[0037] Add gluconic acid and water into a four-necked flask equipped with an electric stirrer, a constant pressure dropping funnel, a thermometer and a reflux condenser, heat to 70°C, stir for 15 minutes, add trisodium phosphate and benzotriazole dropwise, and heat up To 90°C, react for 3h.
[0038] Add ethylenediamine, water-soluble copper sulfide, polyaspartic acid and sodium hypophosphite, raise the temperature to 110°C, and react for 3 hours.
[0039] Raise the temperature to 130°C, add the remaining raw materials, stir for 70 minutes, cool to room temperature and discharge to obtain ...
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