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A solvent-free internal drag-reducing coating and its preparation method

A solvent-free, coating technology, applied in anti-corrosion coatings, fire-retardant coatings, epoxy resin coatings, etc., can solve the problem that the internal drag reduction coatings cannot meet the requirements of thin coating, flexibility and short-term heat resistance, and salt spray resistance at the same time. It has high requirements on salt water immersion performance, poor flexibility and heat resistance, etc., to achieve good salt spray resistance, good salt water immersion performance, and no need for special equipment.

Active Publication Date: 2020-08-18
BC P INC CHINA NAT PETROLEUM CORP +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, solvent-based internal drag-reducing coatings are mostly used in large-scale gas pipelines. However, solvent-based coatings have the problems of being harmful to the human body, polluting the environment, and wasting solvents. Solvent-free coatings are often suitable for thick coatings due to their high viscosity. Coating, it is difficult to obtain a thin coating with good appearance, and the molecular chain length of the main film-forming resin is short, and the flexibility and heat resistance are poor
Solvent-free coatings will become the development trend of internal drag-reducing coatings, but the existing solvent-free coatings cannot meet the requirements of thin coating, flexibility and short-term heat resistance of internal drag-reducing coatings at the same time. Coatings have high requirements on salt spray resistance and salt water immersion resistance, so the performance of drag-reducing coatings in steel gas pipelines is gradually put forward higher and higher requirements

Method used

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  • A solvent-free internal drag-reducing coating and its preparation method

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preparation example Construction

[0050] On the other hand, based on the same inventive concept, the embodiment of the present application provides a method for preparing the above-mentioned solvent-free internal drag-reducing coating, such as figure 1 As shown, it specifically includes the following steps:

[0051] Step S110: Mix 1 part by weight of epoxy resin, 0.1-0.4 parts by weight of modified flexible epoxy resin, 0.1-0.2 parts by weight of toughening agent, and 0.1-0.15 parts by weight of reactive diluent, and then add 0.01 ~0.02 parts by weight of defoaming and defoaming agent, 0.01~0.03 parts by weight of leveling agent, 0.02~0.03 parts by weight of dispersant, 0.01~0.1 parts by weight of thixotropic anti-settling agent, and then add 0.7~1.3 parts by weight Corrosion-resistant pigments and fillers in parts by weight are dispersed and ground to obtain component A;

[0052] Step S120: Mix 1 part by weight of modified polyamide resin, 0.1-0.3 parts by weight of modified aromatic amine resin, and 0.02-0....

Embodiment 1

[0060] 1 weight part of low viscosity epoxy resin E54, 0.3 weight part of modified flexible epoxy resin (EPIKOTE 874L-X-90), 0.10 weight part of phthaloyl polyether ketone, 0.1 weight part Parts of isomerized monocarboxylic acid glycidyl ester (CARDURA E-10P) was dispersed and dissolved, and then 0.01 parts by weight of defoaming and defoaming agent (BYK-A530), 0.02 parts by weight of fluorocarbon modified polyacrylic acid leveling agent were added (AFCONA-3777), 0.02 parts by weight of low molecular weight unsaturated carboxylic acid polymer high-efficiency dispersant (BYK-P104S) high-speed dispersion, while stirring, add 0.01 parts by weight of modified fumed silica (Degussa fumed silica Silicon R972), 0.2 parts by weight of 800 mesh quartz powder, 0.3 parts by weight of 800 mesh wollastonite powder, 0.3 parts by weight of talc powder of 800 mesh and 0.3 parts by weight of iron oxide red, stirred at high speed for 0.5h, and ground for 0.5h with a sand mill. Filtrate the mate...

Embodiment 2

[0062] 1 weight part of low-viscosity epoxy resin E54, 0.2 weight part of modified flexible epoxy resin (EPIKOTE 874L-X-90), 0.10 weight part of phthaloyl polyether ketone, 0.1 weight part Parts of isomeric monocarboxylic acid glycidyl ester (CARDURA E-10P) were dispersed and dissolved, and then 0.02 parts by weight of defoaming and defoaming agent (BYK-A530), 0.02 parts by weight of fluorocarbon modified polyacrylic acid leveling agent ( AFCONA-3777), 0.03 parts by weight of low molecular weight unsaturated carboxylic acid polymer high-efficiency dispersant (BYK-P104S) high-speed dispersion, while stirring, add 0.03 parts by weight of modified fumed silica (Degussa fumed silica R972 ), 0.2 parts by weight of 800 mesh quartz powder, 0.3 parts by weight of 800 mesh wollastonite powder, 0.3 parts by weight of 800 mesh talcum powder and 0.3 parts by weight of iron oxide red, after stirring at high speed for 0.5h, grind 1h with a sand mill, and filter the material Prepare a mixed ...

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Abstract

The invention discloses a solvent-free internal drag reducing coating and a preparation method thereof, and belongs to the technical field of coating chemical industry. The coating is composed of a component A and a component B. The component A comprises the raw materials in parts by weight: 1 part of epoxy resin, 0.1-0.4 part of modified flexible epoxy resin, 0.1-0.2 part of a toughening agent 0.1-0.15 part of an active diluent, 0.01-0.02 part of a defoaming and de-aeration agent, 0.01-0.03 part of a leveling agent, 0.02-0.03 part of a dispersant, 0.01-0.1 part of a thixotropic anti-settlingagent, and 0.5-0.9 part of corrosion-resistant pigments and fillers. The component B comprises the raw materials in parts by weight: 1 part of modified polyamide resin, 0.1-0.3 part of modified aromatic amine resin, 0.02-0.06 part of a curing agent, 0.01-0.05 part of a dispersant, 0.01-0.05 part of a thixotropic agent and 0.4-0.9 part of corrosion-resistant pigments and fillers. The weight ratio of the component A to the component B is 1 to (0.8-0.9). The coating can meet the requirements of thin coating property, flexibility, short-term heat resistance and salt spray resistance property at the same time.

Description

technical field [0001] The invention relates to the technical field of coating chemical industry, in particular to a solvent-free internal drag-reducing coating and a preparation method thereof. Background technique [0002] The drag-reducing coating in the gas pipeline can greatly reduce the friction coefficient of gas transmission, increase the gas transmission volume, and improve the transmission efficiency while it has an anti-corrosion effect on the metal pipeline. be applied on a large scale. At present, solvent-based internal drag-reducing coatings are mostly used in large-scale gas pipelines. However, solvent-based coatings have the problems of being harmful to the human body, polluting the environment, and wasting solvents. Solvent-free coatings are often suitable for thick coatings due to their high viscosity. Coating, it is difficult to obtain a thin coating with good appearance, and the molecular chain length of the main film-forming resin is short, and the flex...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D163/00C09D179/08C09D5/08C09D7/65C08G59/54
CPCC08G59/54C08K2003/2272C08L2201/08C08L2205/025C08L2205/035C09D5/084C09D5/18C09D163/00C09D179/08C08L79/08C08L63/00C08L71/00C08K3/22C08K3/36C08K3/34
Inventor 崔灿灿郭晓军韩忠智王磊丁超李石刘杨宇刘本华林竹段绍明
Owner BC P INC CHINA NAT PETROLEUM CORP
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