Nano heat-insulation coating layer applied to hollow glass
A nano-insulation and glass technology, applied in coatings and other directions, can solve the problems of large-scale application of insulating glass, increase of indoor lighting energy consumption, decrease of visible light transmittance, etc., to achieve excellent adhesion performance and good spectral selection. The effect of strong resistance and hardness
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Embodiment 1
[0017] A kind of nano heat-insulating coating applied on the insulating glass, the nano-composite material that mass fraction accounts for 0.75% is added in the acrylic emulsion coating, the preparation method of this nano-composite material comprises the following steps:
[0018] (1) Weigh 0.8 moles of aluminum trichloride hexahydrate and 0.3 moles of aluminum nitrate, add them to 500 ml of deionized water, stir for 50 minutes, add 5.0 ml of 30% ammonium carbonate solution, mix and stir for 20 minutes, then add In a three-necked flask containing a thermometer and a stirrer, heat the oil bath to 60°C;
[0019] (2) Heat the reaction for 1 hour to obtain a precipitate, pass nitrogen gas, slowly add ammonia water dropwise at a stirring speed of 700 rpm to adjust the pH value of the reaction system to 9.6, continue stirring for 40 minutes, stop, and age at 40°C After 2.0 hours, add 1.5 grams of acetone and 2.0 grams of polyethylene glycol and continue stirring for 25 minutes;
[...
Embodiment 2
[0026] A kind of nano-insulation coating applied on hollow glass, the nano-composite material that mass fraction accounts for 0.78% is added in acrylic emulsion coating, the preparation method of this nano-composite material comprises the following steps:
[0027] (1) Weigh 0.85 moles of aluminum trichloride hexahydrate and 0.4 moles of aluminum nitrate, add them to 520 ml of deionized water, stir for 55 minutes, add 5.3 ml of 35% ammonium carbonate solution, mix and stir for 25 minutes, then add In a three-necked flask containing a thermometer and a stirrer, the oil bath is heated to 62°C;
[0028] (2) Heat the reaction for 1.5 hours to obtain a precipitate, pass through nitrogen, slowly add ammonia water dropwise at a stirring speed of 730 rpm to adjust the pH value of the reaction system to 9.7, continue stirring for 45 minutes, stop, and age at 45°C After 2.5 hours, add 1.8 grams of acetone and 2.3 grams of polyethylene glycol, and continue stirring for 28 minutes;
[002...
Embodiment 3
[0035] A kind of nano heat-insulating coating applied on hollow glass, the nano-composite material that mass fraction accounts for 0.80% is added in acrylic emulsion coating, the preparation method of this nano-composite material comprises the following steps:
[0036] (1) Weigh 0.9 moles of aluminum trichloride hexahydrate and 0.5 moles of aluminum nitrate, add them to 550 ml of deionized water, stir for 60 minutes, add 5.5 ml of 40% ammonium carbonate solution, mix and stir for 30 minutes, then add In a three-necked flask containing a thermometer and a stirrer, heat the oil bath to 65°C;
[0037] (2) Heat the reaction for 2 hours to obtain a precipitate, pass nitrogen gas, slowly add ammonia water dropwise at a stirring speed of 750 rpm to adjust the pH value of the reaction system to 9.8, continue stirring for 50 minutes, stop, and age at 50°C After 3.0 hours, add 2.0 grams of acetone and 2.5 grams of polyethylene glycol and continue stirring for 30 minutes;
[0038](3) Co...
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