Method for preparing melamine resin finishing agent
A technology of melamine resin and finishing agent, which is applied in microsphere preparation, microcapsule preparation, fiber treatment and other directions, can solve the problems of short fragrance retention time, low fragrance encapsulation rate, low mechanical strength of capsule wall, etc. The effect of simplifying the finishing process
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
preparation example Construction
[0034] (3) Preparation of melamine resin prepolymer
[0035] Put 5-10 parts of melamine and 10-20 parts of 37% formaldehyde solution into a four-necked bottle in parts by weight, heat up to 60-80°C under stirring conditions, and add 0.1-1 part of triethanolamine after the melamine is completely dissolved, Adjust the pH to 7-10, and react for 10-30 minutes to obtain a transparent and viscous melamine resin prepolymer;
[0036] (4) Preparation of self-adhesive double-wall essence microcapsules
[0037] By weight, 10-30 parts of essence, 2-5 parts of methyl methacrylate, 2-5 parts of acrylonitrile, 1-3 parts of butyl acrylate, 1-3 parts of isooctyl acrylate, 0.2-0.5 parts of methyl Acrylic acid, 0.2-0.5 parts of hydroxyethyl acrylate, 0.1-0.3 parts of diacetone acrylamide, 0.1-0.3 parts of adipic acid dihydrazide, and 0.02-0.05 parts of azobisisobutyronitrile are placed in a beaker at a temperature of 30 Stir and mix at -50°C to form a homogeneous oil solution;
[0038] Mix th...
Embodiment 1
[0045] (1) Preparation of styrene-maleic anhydride copolymer powder
[0046] Under the condition of nitrogen protection, add monomer maleic anhydride and initiator into the medium to fully dissolve, then add monomer styrene to dissolve in the system, and react at 50°C for 0.5h to obtain high molecular weight styrene and horse The dispersion system of maleic anhydride polymer microspheres is centrifuged and vacuum-dried to obtain a white solid of alternating copolymers of high molecular weight styrene and maleic anhydride;
[0047] Wherein, the initiator is an organic peroxide or an azo compound; the medium is an organic acid alkyl ester, or a mixed solution of a ketone and an alkane;
[0048] The consumption relation of maleic anhydride and styrene, molar ratio is 5: 1, and the mass concentration sum of two kinds of monomer maleic anhydride and styrene in the reaction system is 15%; In the reaction system, the mass concentration of initiator is 0 %; The volume fraction of ket...
Embodiment 2
[0061] (1) Preparation of styrene-maleic anhydride copolymer powder
[0062] Under the condition of nitrogen protection, add monomer maleic anhydride and initiator into the medium to fully dissolve, then add monomer styrene to dissolve in the system, and react at 90°C for 72h to obtain high molecular weight styrene and maleic acid The dispersion system of acid anhydride polymer microspheres is centrifuged and vacuum-dried to obtain a white solid of alternating copolymer of high molecular weight styrene and maleic anhydride;
[0063] Wherein, the initiator is an organic peroxide or an azo compound; the medium is an organic acid alkyl ester, or a mixed solution of a ketone and an alkane;
[0064] The consumption relation of maleic anhydride and styrene is 1: 5 by molar ratio, and the mass concentration sum of two kinds of monomer maleic anhydride and styrene is 43% in the reaction system; The mass concentration of initiator is 0.4 in the reaction system %; The volume fraction o...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com