Stable piezoelectric ceramic and preparation method thereof
A piezoelectric ceramic and stable technology, applied in the field of materials, can solve problems affecting the normal operation of products, material performance deterioration, poor stability, etc., and achieve the effects of easy control operation, small performance drift, and high tensile strength
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Embodiment 1
[0022] In the embodiment of the present invention, a stable piezoelectric ceramic includes the following raw materials: 20 kg of strontium carbonate, 7 kg of lead oxide, 11 kg of mercaptopropionic acid, 11 kg of di-n-octyl phthalate, 1 kg of ocher, 3 kg of zinc oxide, silica fume Stone 3kg.
[0023] Mercaptopropionic acid was mixed with 6 times its mass of deionized water to prepare a mercaptopropionic acid solution. Mix strontium carbonate, lead oxide, ochre, zinc oxide, and wollastonite, grind them, pass through a 120-mesh sieve, then add mercaptopropionic acid solution, heat up to 102°C, and seal and stir at this temperature for 1.8 hours. The stirring speed is 220r / min to prepare mixture A. Put di-n-octyl phthalate into mixture A, raise the temperature to 128°C, and seal and stir at this temperature for 1 hour at a stirring speed of 180r / min, then stop heating and perform ultrasonic treatment for 35min with ultrasonic power of 700W. The precipitate was collected by centr...
Embodiment 2
[0025] In the embodiment of the present invention, a stable piezoelectric ceramic comprises the following raw materials: 30 kg of strontium carbonate, 15 kg of lead oxide, 19 kg of mercaptopropionic acid, 19 kg of di-n-octyl phthalate, 5 kg of ocher, 7 kg of zinc oxide, silica fume Stone 7kg.
[0026] Mercaptopropionic acid was mixed with 8 times its mass of deionized water to prepare a mercaptopropionic acid solution. Mix strontium carbonate, lead oxide, ochre, zinc oxide, and wollastonite, grind them, pass through a 150-mesh sieve, then add mercaptopropionic acid solution, heat up to 102°C, and seal and stir at this temperature for 2 hours at a stirring speed of 220r / min, the mixture A was prepared. Put di-n-octyl phthalate into mixture A, raise the temperature to 128°C, and seal and stir at this temperature for 1.2h at a stirring speed of 180r / min, then stop heating and ultrasonically treat for 35min with an ultrasonic power of 700W , centrifuged to collect the precipita...
Embodiment 3
[0028] In the embodiment of the present invention, a stable piezoelectric ceramic comprises the following raw materials: 22 kg of strontium carbonate, 9 kg of lead oxide, 13 kg of mercaptopropionic acid, 13 kg of di-n-octyl phthalate, 2 kg of ocher, 4 kg of zinc oxide, silica fume Stone 4kg.
[0029] Mercaptopropionic acid was mixed with 7 times its mass of deionized water to prepare a mercaptopropionic acid solution. Mix strontium carbonate, lead oxide, ochre, zinc oxide, and wollastonite, grind them, pass through a 150-mesh sieve, then add mercaptopropionic acid solution, heat up to 102°C, and seal and stir at this temperature for 1.9 hours. The stirring speed is 220r / min to prepare mixture A. Put di-n-octyl phthalate into mixture A, raise the temperature to 128°C, and seal and stir at this temperature for 1.1h at a stirring speed of 180r / min, then stop heating and ultrasonically treat for 35min with an ultrasonic power of 700W , centrifuged to collect the precipitate, was...
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