Silica gel modified desulfurizing agent and preparation method thereof
A desulfurization agent and modification technology, applied in the field of desulfurization agent, can solve the problems of insufficient sulfur capacity and unsatisfactory desulfurization depth, etc., and achieve the effects of enhanced desulfurization effect, more recycling times, and good adsorption performance
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Embodiment 1
[0026] A silica gel modified desulfurizer, which is made up of the following raw materials in parts by weight:
[0027] Ethyl orthosilicate 230, aluminum dihydrogen phosphate 4, polyvinyl alcohol 2, ethylene bisstearamide 1, tetrabutyl titanate 20, cyanoethyl cellulose 3, lime powder 5, sodium myristate soap 3 , Potassium Monododecyl Phosphate 1, Palm Wax 3, Ammonium Ferrous Sulfate 0.2, Dibutyltin Dilaurate 1, Trimethylolpropane 2, Barium Stearate 4, 1-Hydroxyethyl-2-Oil Base imidazoline 1, tin dioxide 8.
[0028] A preparation method of silica gel modified desulfurizer, comprising the following steps:
[0029] (1) Take palm wax, add it to 8 times its weight in dichloromethane, put it into an oil bath with a temperature of 120°C, keep it warm and stir for 10 minutes, add barium stearate, stir to normal temperature, and get dichloromethane solution;
[0030] (2) Get trimethylolpropane, join in the dimethylformamide of its weight 10 times, stir evenly, obtain alkyl amide sol...
Embodiment 2
[0038] A silica gel modified desulfurizer, which is made up of the following raw materials in parts by weight:
[0039] Ethyl Orthosilicate 26, Aluminum Dihydrogen Phosphate 3, Polyvinyl Alcohol 1, Ethylene Bis Stearamide 0.7, Tetrabutyl Titanate 15, Cyanoethyl Cellulose 2, Lime Powder 3, Sodium Myristate Soap 2 -3. Potassium monododecyl phosphate 0.8, Palm wax 2-3, Ferrous ammonium sulfate 0.1, Dibutyltin dilaurate 0.5, Trimethylol propane 1, Barium stearate 2, 1-Hydroxyethyl -2-oleyl imidazoline 0.7, tin dioxide 5.
[0040] A preparation method of silica gel modified desulfurizer, comprising the following steps:
[0041] (1) Take palm wax, add it to 6 times its weight in dichloromethane, put it into an oil bath with a temperature of 110°C, keep it warm and stir for 7 minutes, add barium stearate, and stir to normal temperature to get dichloromethane solution;
[0042] (2) Get trimethylolpropane, join in the dimethylformamide of its weight 6 times, stir evenly, obtain alky...
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