HPLC (high-performance liquid chromatography) fingerprint spectrum measurement method for standard Yunujian decoction
A standard fingerprint and fingerprint technology, which is applied in the field of HPLC fingerprint determination of Yunujian standard soup, can solve problems such as lack of quality control, reduce the possibility of manual processing, have good stability, and ensure the stability of chemical composition. The effect of safety in use
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Embodiment 1
[0071] Example 1 The HPLC Fingerprint Determination Method of Yunu Decoction Standard Decoction
[0072] 1.1 Instruments and reagents
[0073] instrument:
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[0076] Reagent:
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[0078] Control substance:
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[0080] 1.2 Sample preparation:
[0081] 1.2.1 Preparation of samples and sample solutions for testing
[0082] (1) Sample preparation: take different origins and different batches of medicinal materials or decoction pieces that have passed the inspection of the Chinese Pharmacopoeia, weigh 15g of raw gypsum, 15g of rehmannia glutinosa, 6g of Radix Ophiopogon japonicus, 4.5g of Zhimu, 4.5g of Achyranthes bidentata, add 300mL Soak in deionized water for 60 minutes, boil with strong fire (220V) for 10 minutes, decoct with slow fire (140V) for 35 minutes (the amount of decoction is about 140mL), pour it while it is hot, and make the standard soup of Yunujian.
[0083] (2) Preparation of the test sample solution: Take 5 mL of the ...
Embodiment 2
[0193] Example 2 The quality control method of standard granules of Yunu decoction
[0194] A kind of quality control method of standard granule of jade female decoction, comprises the following steps:
[0195] (1) According to the method in 1.2.1 (1) in Example 1, prepare the Jade Girl Fried Standard Soup, adopt the assay method in Example 1 to set up the standard fingerprint of the Jade Girl Fried Standard Soup;
[0196] (2) Get the standard granules of Yunujian to be checked, and obtain fingerprints according to the assay method in Example 1;
[0197] (3) Compare the fingerprints obtained in step (2) with the standard fingerprints obtained in step (1), if they meet, they are qualified products, and if they do not meet, they are unqualified products.
[0198] Preparation of the test sample solution of the standard granules of Yunujian: take the standard granules of Yunujian under the difference in filling volume, mix them evenly, grind them finely, take 1.5g, accurately wei...
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