A method for rapid determination of sulfonamides and quinolones residues in eggs
A rapid determination technology for quinolones, applied in the field of egg sample detection, can solve the problems of liquid chromatography-mass spectrometry/mass spectrometry of sulfa drugs that have not been reported in the literature, and achieve the effect of improving detection sensitivity, improving sensitivity and reducing errors
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[0018] In order to make the technical means, creative features, goals and effects achieved by the present invention easy to understand, the present invention will be further described below in conjunction with specific embodiments.
[0019] This embodiment adopts the following technical solutions: a method for quickly measuring sulfonamides and quinolones drug residues in eggs, the steps of which are:
[0020] (1) Prepare materials and reagents: QuEChERS EMR-Lipid rapid extraction tube, acetonitrile, methanol, formic acid (all HPLC pure reagents), distilled water, and target analytes: sulfathiazole (ST), sulfamethoxazole (SIZ ), sulfadoxine (SDM'), sulfamethazine (SM1), sulfachloropyridazine (SCP), sulfapyridine (SPD), sulfamethiadiazole (SMT), sulfamethoxypyridazine (SMP), Sulfadiazine (SD), Sulfamethoxine (SMM), Sulfadesoxine (SDM), Sulfamethoxazole (SMZ), Sulfaquinoxaline (SQ), Sulfamethazine (SM2), Mabosa Star, lomefloxacin, pefloxacin, enrofloxacin, sarafloxacin, ofloxac...
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