Terylene cleanroom clothes fabric coating adhesive and preparation method thereof
A technology of clean clothes and coating glue, which is applied in the fields of biochemical fiber treatment, fiber type, textiles and papermaking, etc., to achieve the effects of improving dust filtration, enhancing film-forming performance, and excellent washing resistance
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Embodiment 1
[0027] Add diphenylmethane diisocyanate (MDI) 50, polyethylene glycol 10 with an average molecular weight of 1450, polyethylene glycol 15 with an average molecular weight of 1000, and polybutadiene glycol 50 with an average molecular weight of 2000. 75°C, react for 2.5 hours, then cool down to 50°C, add styrene 10, neoprene rubber 10, methacryloyloxyethyltrimethylammonium chloride 5, deionized water 150, heat up to 75°C, add dropwise The mixed solution containing the initiator 2,2'-azodiisobutylamidine dihydrochloride 1 and deionized water 10 was added dropwise for 2 hours, then kept at 80°C for 1 hour, cooled to 45°C and discharged. Acrylic modified polyurethane emulsion;
[0028] The acrylic modified polyurethane emulsion 100 prepared above was added with polyurethane leveling rheology agent 2 and blocked isocyanate crosslinking agent 2, stirred evenly, and filtered to obtain a product with a viscosity of 3500 mPa·s.
Embodiment 2
[0030] Add diphenylmethane diisocyanate (MDI) 60, polyethylene glycol 12 with an average molecular weight of 1450, polyethylene glycol 16 with an average molecular weight of 1000, and polybutadiene diol 55 with an average molecular weight of 2000. 70 ° C, react for 2.6 hours, then cool down to 55 ° C, add styrene 12, neoprene rubber 15, methacryloyloxyethyl trimethyl ammonium chloride 6, deionized water 180, heat up to 70 ° C, add dropwise The mixed solution containing initiator 2,2'-azodiisobutylamidine dihydrochloride 1.5 and deionized water 15 was added dropwise for 2.2 hours, then kept at 81°C for 1 hour, cooled to 45°C and discharged to obtain Acrylic modified polyurethane emulsion;
[0031] The acrylic modified polyurethane emulsion 100 prepared above was added with polyurethane leveling rheology agent 3 and blocked isocyanate crosslinking agent 2.5, stirred evenly, and filtered to obtain a product with a viscosity of 3650 mPa·s.
Embodiment 3
[0033] Add diphenylmethane diisocyanate (MDI) 65, polyethylene glycol 14 with an average molecular weight of 1450, polyethylene glycol 18 with an average molecular weight of 1000, and polybutadiene glycol 58 with an average molecular weight of 2000. 78°C, react for 2.8 hours, then cool down to 56°C, add styrene 16, neoprene rubber 17, methacryloyloxyethyltrimethylammonium chloride 8, deionized water 190, heat up to 78°C, add dropwise The mixed solution containing initiator 2,2'-azobisisobutylamidine dihydrochloride 1.8 and deionized water 18 was added dropwise for 2.3 hours, then kept at 83°C for 1 hour, cooled to 45°C and discharged to obtain Acrylic modified polyurethane emulsion;
[0034] The acrylic modified polyurethane emulsion 100 prepared above was added with polyurethane leveling rheology agent 4 and blocked isocyanate crosslinking agent 3, stirred evenly, and filtered to obtain a product with a viscosity of 3800 mPa·s.
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