A device and method for microwave-assisted excitation to suppress the self-absorption effect of laser-induced breakdown spectrum
A laser-induced breakdown and self-absorption effect technology, applied in the field of plasma emission spectroscopy, can solve the problems of OPO wavelength tunable lasers such as expensive, cumbersome operation, and difficult maintenance, so as to simplify the process of loading samples and avoid self-absorption , Improve the effect of accuracy and precision
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Embodiment 1
[0045] In this embodiment, the method is described in detail by taking the detection of sodium element in a sodium chloride powder tablet sample as an example.
[0046] The laser 1 used in this experiment is Leibao Vlite-200Nd:YAG laser, the laser wavelength is 1064nm, the laser energy is 40mJ, and the laser repetition frequency is 1Hz. The integration time of the device 9 is 2ms, the delay time is 2us, and the average is 2 times; the power of the microwave generator 15 is 120W.
[0047] In the first step, the sodium chloride powder is made into a disc with a diameter of 40 mm and a thickness of 4 mm by a tablet machine under a pressure of 20 MPa. After placing the sample, adjust the optical path so that the focus position of the converging lens 4 is located at 4 mm below the sample;
[0048] In the second step, the microwave probe is positioned 2 mm above the sample surface, and a microwave probe with a double-needle structure is used. The distance between the double needles ...
Embodiment 2
[0053] In order to verify whether the present invention has the effect of simultaneously inhibiting the self-absorption of multiple elements, this embodiment takes the simultaneous detection of sodium and potassium in a potassium feldspar (GBW03116) tablet sample as an example to describe the method in detail.
[0054] The laser 1 used in this experiment is Leibao Vlite-200Nd:YAG laser, the laser wavelength is 1064nm, the laser energy is 40mJ, and the laser repetition frequency is 1Hz. The integration time of the device 9 is 2ms, the delay time is 2us, and the average is 2 times; the power of the microwave generator 15 is 100W.
[0055] In the first step, the potassium feldspar powder is made into a disc with a diameter of 40mm and a thickness of 4mm by a tablet machine under a pressure of 20MPa. After placing the sample, adjust the optical path so that the focal position of the converging lens 4 is located at 4mm below the sample, and then open the The pulse laser outputs a l...
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