Preparation method and application of copper sulphide nano-material
A nanomaterial and nanocomposite material technology, which is applied in the field of preparation of BSA-CuS nanocomposite materials, can solve the problems of ecosystem hazards, non-degradability of graphene oxide and unknown toxicity, high cost, and cost limitations, and achieves low bactericidal dose, Low pressure and low cost effect
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Embodiment 1
[0029] A preparation method of BSA-CuS nanocomposite material, comprising the following steps:
[0030] (1) Add 5 ml of 10 mM Cu(NO 3 ) 2 The solution was added to 5 mL bovine serum albumin BSA solution with a concentration of 5 mg / mL, and stirred at room temperature for 30 min to obtain a BSA-Cu suspension in which BSA-Cu conjugates were formed, and the color of the solution was light blue.
[0031] (2) Adjust the pH of the BSA-Cu suspension obtained in step (1) to 3.0 with a 95% nitric acid solution, add 0.5ml of a 0.5 M thioacetamide solution, and the solution becomes pale after shaking. yellow. The above solution was placed in a constant temperature water bath at 90 °C for natural incubation for 1 h to prepare BSA-CuS nanocomposites.
Embodiment 2
[0033] The BSA-CuS nanocomposite material gained in embodiment one is carried out TEM characterization, the result is as follows figure 1 As shown, the average particle size of CuS nanoparticles is around 50 nm.
Embodiment 3
[0035] The BSA-CuS nanocomposite obtained in Example 1 was subjected to ultraviolet spectrum detection before and after near-infrared light irradiation, and the results figure 2 As shown, the prepared BSA-CuS nanocomposites have characteristic absorption peaks in the near-infrared region, indicating that the BSA-CuS nanocomposites synthesized by the present invention have stable photothermal conversion efficiency.
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