Core-shell ceramic microspheres and preparation method thereof
A ceramic microsphere, core-shell technology, applied in the field of SiO2/SiCN core-shell ceramic microsphere and its preparation
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Embodiment 1
[0035] Add 0.5 g of silicon dioxide and 5 mL of absolute ethanol into the three-necked flask, and put it into an ultrasonic instrument for sufficient ultrasonic dispersion for 15 minutes. Add 0.5 mL of silane coupling agent MPS, and react in a water bath at 40° C. for 24 h. Centrifugal washing, drying. Disperse the modified silica in an aqueous phase system containing 0.1 g of emulsifier OP-100, 7.5 g of deionized water, and 7.5 g of acetonitrile, and add 1 g of polysilazane dropwise to the above aqueous phase system. 0.01ml per minute, ultrasonically dispersed to obtain a uniform emulsion, cross-linked and solidified in an autoclave at 160°C for 4 hours, after the reaction, it was centrifuged and washed three times, dried at 80°C, and then placed in a vacuum furnace for sintering. From room temperature 20 degrees Celsius, the temperature is raised to 1000 degrees Celsius at a rate of 5 degrees Celsius per minute and kept for 5 hours and then cooled to room temperature 20 deg...
Embodiment 2
[0037] Add 0.5 g of silicon dioxide and 5 mL of absolute ethanol into the three-necked flask, and put it into an ultrasonic instrument for sufficient ultrasonic dispersion for 15 minutes. Add 0.5 mL of silane coupling agent MPS, and react in a water bath at 40° C. for 24 h. Centrifugal washing, drying. Disperse the modified silicon dioxide in an aqueous phase system containing 0.2 g of emulsifier OP-100, 15 g of deionized water, and 15 g of acetonitrile, and add 2 g of polysilazane dropwise to the above aqueous phase system at a rate of Minute 0.05ml, ultrasonic dispersion to obtain a homogeneous emulsion, cross-linked and solidified in an autoclave at 200 ° C for 4 hours, after the reaction, it was centrifuged and washed three times, dried at 80 ° C, placed in a vacuum furnace for sintering, from room temperature Start at 25 degrees Celsius and heat up to 1600 degrees Celsius at a rate of 2 degrees Celsius per minute and keep it warm for 1 hour and then cool to room temperat...
Embodiment 3
[0039] Add 0.5 g of silicon dioxide and 5 mL of absolute ethanol into the three-necked flask, and put it into an ultrasonic instrument for sufficient ultrasonic dispersion for 15 minutes. Add 0.5 mL of silane coupling agent MPS, and react in a water bath at 40° C. for 24 h. Centrifugal washing, drying. Disperse the modified silicon dioxide in an aqueous phase system containing 0.2 g of emulsifier OP-10, 15 g of deionized water, and 15 g of acetonitrile, and add 2 g of polysilazane dropwise to the above aqueous phase system at a rate of 0.03ml per minute, ultrasonic dispersion to obtain a homogeneous emulsion, cross-linked and solidified in an autoclave at 200°C for 6 hours, after the reaction, it was centrifuged and washed three times, dried at 80°C, and then placed in a vacuum furnace for sintering. At room temperature of 20 degrees Celsius, the temperature is raised to 1200 degrees Celsius at a rate of 4 degrees Celsius per minute and kept for 3 hours, then cooled to room t...
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