A kind of manufacturing method of cucr alloy with large size, high density and high uniformity
A manufacturing method and high-density technology, applied in the manufacturing field of copper-based vacuum contact materials, to achieve the effects of improving current density distribution, simple process, and accelerating gas emission
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Embodiment 1
[0033] The large-scale CuCr alloy of present embodiment is carried out as follows:
[0034] Step 1. Weigh 7.0kg of Cu powder and 3.0kg of Cr powder respectively, and mix them for 10 hours by mechanical mixing method to obtain uniform CuCr mixed powder; weigh 3.35kg of CuCr mixed powder for sintering;
[0035] Step 2. Fill the weighed CuCr mixed powder into the graphite mold; use a manual hydraulic press to pre-press the graphite mold filled with the CuCr mixed powder, and the pressure is ~ 10MPa;
[0036] Step 3. Wrap ~5mm thick carbon felt on the periphery of the graphite mold with CuCr mixed powder, then place it in the furnace of the spark plasma sintering system, evacuate it to below 5Pa, and feed DC pulse current to mix CuCr The powder is consolidated and formed, and the process conditions are:
[0037] The axial pressure is 30MPa;
[0038] The heating rate is 15°C / min (≤300°C) and 35°C / min (>300°C);
[0039] The sintering temperature is 850°C;
[0040] The holding ti...
Embodiment 2
[0043] The large-scale CuCr alloy of present embodiment is carried out as follows:
[0044] Step 1. Weigh 14.0kg of Cu powder and 6.0kg of Cr powder respectively, and mix them by mechanical mixing method for 10h to obtain uniform CuCr mixed powder; weigh 5.66kg of CuCr mixed powder for sintering;
[0045] Step 2. Fill the weighed CuCr mixed powder into the graphite mold; use a manual hydraulic press to pre-press the graphite mold filled with the CuCr mixed powder, and the pressure is ~ 10MPa;
[0046] Step 3. Wrap ~5mm thick carbon felt on the periphery of the graphite mold with CuCr mixed powder, then place it in the furnace of the spark plasma sintering system, evacuate it to below 5Pa, and feed DC pulse current to mix CuCr The powder is consolidated and formed, and the process conditions are:
[0047] The axial pressure is 60MPa;
[0048] The heating rate is 10°C / min (≤300°C) and 30°C / min (>300°C);
[0049] The sintering temperature is 800°C;
[0050] The holding time i...
Embodiment 3
[0053] The large-scale CuCr alloy of present embodiment is carried out as follows:
[0054] Step 1. Weigh 7.0kg of Cu powder and 3.0kg of Cr powder respectively, and mix them for 10 hours by mechanical mixing method to obtain uniform CuCr mixed powder; weigh 655g of CuCr mixed powder for sintering;
[0055] Step 2. Fill the weighed CuCr mixed powder into the graphite mold; use a manual hydraulic press to pre-press the graphite mold filled with the CuCr mixed powder, and the pressure is ~ 10MPa;
[0056] Step 3. Wrap ~5mm-thick carbon felt around the graphite mold with CuCr mixed powder, then place it in the furnace of the spark plasma sintering system, evacuate it to below 5Pa, and then pass a DC pulse current to the CuCr The mixed powder is consolidated and formed, and the process conditions are:
[0057] The axial pressure is 10MPa;
[0058] The heating rate is 20°C / min (≤300°C) and 50°C / min (>300°C);
[0059] The sintering temperature is 880°C;
[0060] The holding time...
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