Sound-insulation and heat-insulation hollow-glass spacing bar and preparation method thereof
A spacer, glass technology, applied in the improvement of windows/doors, building components, climate change adaptation, etc., can solve the problems of affecting the perspective of insulating glass, condensation, shortening of service life, etc., and is suitable for large-scale industrial application. , good heat insulation effect, good sound insulation effect
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Embodiment 1
[0020] (1) Weigh 14 parts of polydimethylsiloxane, 5 parts of hexamethyldisiloxane, 4 parts of cyclomethicone, 4 parts of vinyltriethoxysilane, 4 parts of sodium acrylate, 3 parts of n-butyl nitrate, 2 parts of ethyl chloroformate, 5 parts of white carbon black, 4 parts of chloroisopentane, 5 parts of 3-hydroxy-2 butanone, 2 parts of sodium bisulfite, 4 parts of maleic anhydride , 1 part of benzoyl chloride, 2 parts of copper chloride, 1 part of sulfamic acid, 3 parts of sodium ethoxide, 5 parts of sodium metaaluminate, 4 parts of diisooctyl phthalate;
[0021] (2) Add polydimethylsiloxane, hexamethyldisiloxane, cyclomethicone, vinyltriethoxysilane, and sodium acrylate to a high-speed mixer and preheat to 220°C, stir and mix 30 minutes, the stirring speed is 1500 rpm, then add n-butyl nitrite, ethyl chloroformate, chloroisopentane, 3-hydroxy-2 butanone in turn, vacuumize, vacuum sintering, the sintering temperature is 820 ° C, The sintering time is 3 hours to obtain a vacuum ...
Embodiment 2
[0028] (1) Weigh 15 parts of polydimethylsiloxane, 7 parts of hexamethyldisiloxane, 5 parts of cyclomethicone, 5 parts of vinyltriethoxysilane, 5 parts of sodium acrylate, 4 parts of n-butyl nitrate, 3 parts of ethyl chloroformate, 7 parts of white carbon black, 5 parts of chloroisopentane, 6 parts of 3-hydroxy-2 butanone, 2 parts of sodium bisulfite, 5 parts of maleic anhydride , 2 parts of benzoyl chloride, 2 parts of copper chloride, 2 parts of sulfamic acid, 4 parts of sodium ethoxide, 6 parts of potassium pyroantimonate, 5 parts of diethyl phthalate;
[0029] (2) Add polydimethylsiloxane, hexamethyldisiloxane, cyclomethicone, vinyltriethoxysilane, and sodium acrylate to a high-speed mixer and preheat to 220°C, stir and mix 30 minutes, the stirring speed is 1600 rpm, then add n-butyl nitrite, ethyl chloroformate, chloroisopentane, 3-hydroxy-2 butanone in turn, vacuumize, vacuum sintering, the sintering temperature is 830 °C, The sintering time is 3 hours to obtain a vacuu...
Embodiment 3
[0036] (1) Weigh 17 parts of polydimethylsiloxane, 9 parts of hexamethyldisiloxane, 8 parts of cyclomethicone, 8 parts of vinyltriethoxysilane, 6 parts of sodium acrylate, 5 parts of n-butyl nitrate, 6 parts of ethyl chloroformate, 9 parts of white carbon black, 5 parts of chloroisopentane, 6 parts of 3-hydroxy-2 butanone, 3 parts of sodium bisulfite, 7 parts of maleic anhydride , 2 parts of benzoyl chloride, 3 parts of copper chloride, 3 parts of sulfamic acid, 4 parts of sodium ethoxide, 7 parts of aluminum sulfate, 5 parts of dioctyl adipate;
[0037] (2) Add polydimethylsiloxane, hexamethyldisiloxane, cyclomethicone, vinyltriethoxysilane, and sodium acrylate to a high-speed mixer and preheat to 220°C, stir and mix 30 minutes, the stirring speed is 1700 rpm, then add n-butyl nitrite, ethyl chloroformate, chloroisopentane, 3-hydroxy-2 butanone in turn, vacuumize, vacuum sintering, the sintering temperature is 850 °C, The sintering time is 3 hours to obtain a vacuum sintered...
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