Preparation method of CDs/TiO2 composite material, production method of modified EVA film, and application of modified EVA film
A composite material and modification technology, applied in chemical instruments and methods, water/sludge/sewage treatment, chemical/physical processes, etc.
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Embodiment 1
[0052] A CDs / TiO 2 The preparation method of composite material, comprises the following steps:
[0053] (1) After grinding the melon seed shells, place them in a muffle furnace, calcinate them at 300°C for 4 hours, take them out after cooling, and grind them into powder. Take 1.0g of powder in a beaker, add 50mL of water and sonicate for 1h. After the solution obtained by ultrasound is filtered through a 0.22 μm filter membrane, it is centrifuged on a high-speed centrifuge at 12000 r / min for 10 minutes, the supernatant is taken, and the supernatant is bagged with a dialysis bag (MWCO=3500) and placed in twice distilled water for dialysis In two days, the water was changed every 6 hours on average to obtain CDs solution; the ultraviolet absorption spectrum and fluorescence spectrum of CDs were as follows: figure 1 Shown; TEM pictures of CDs as figure 2 shown.
[0054] (2) One-step synthesis of nano-CDs / TiO under hydrothermal conditions 2 composite material. 2.0mL TiCl ...
Embodiment 2
[0060] A CDs / TiO 2 The preparation method of composite material, comprises the following steps:
[0061] (1) After grinding the melon seed shells, place them in a muffle furnace, calcinate them at 250°C for 3 hours, take them out after cooling, and grind them into powder. Take 2.0g of powder in a beaker, add 50mL of water and sonicate for 30min. After filtering the solution obtained by ultrasound through a 0.22 μm filter membrane, centrifuge it on a high-speed centrifuge at 10,000 r / min for 10 minutes, take the supernatant, pack the supernatant with a dialysis bag (MWCO=3500) and put it into twice distilled water for dialysis In two days, the water was changed once every 6 hours on average to obtain the CDs solution; the absorption spectrum and fluorescence spectrum of CDs were as follows: Figure 9 Shown; TEM pictures of CDs as Figure 10 shown.
[0062] (2) One-step synthesis of nano-CDs / TiO under hydrothermal conditions 2 composite material. 2.0mL TiCl 4 Add 2.0mL of...
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