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Ultraviolet curing transfer adhesive for glass substrate

A glass substrate, ultraviolet light technology, applied in the field of transfer adhesive, can solve the problems of poor adhesion of glass substrates, poor chemical corrosion performance, poor boiling resistance, etc., and achieves improved boiling resistance, strong reactivity, phase Good capacitive effect

Active Publication Date: 2017-01-04
SUZHOU BETELY POLYMER MATERIALS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] There are three technical problems in the existing UV-curable transfer adhesives, ①Poor adhesion on glass substrates
② Poor boiling resistance on glass substrates
③Poor chemical corrosion resistance such as alcohol and ethyl acetate on the glass substrate

Method used

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  • Ultraviolet curing transfer adhesive for glass substrate
  • Ultraviolet curing transfer adhesive for glass substrate
  • Ultraviolet curing transfer adhesive for glass substrate

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] A method for preparing a UV-curable transfer adhesive for a glass substrate, comprising the following steps:

[0040] In parts by weight, 30 parts of nine-dimensional commercial trifunctional resin UA-787LV containing carboxyl groups, 13 parts of isobornyl acrylate reactive diluent, 1 part of 2,4,6-trimethylbenzoyl-di Phenylphosphine oxide, 3 parts of 1-hydroxy-cyclohexyl-phenyl ketone, and 3 parts of 2-hydroxyethyl methacrylate phosphate additives were sequentially added into the stirring disperser. In a dry and ventilated environment, stir at 1000 rpm for 4 hours, stir and disperse evenly, filter out impurities, keep away from light, and seal the package as the main ingredient;

[0041] In parts by weight, 8 parts of 2-hydroxyethyl acrylate, 2 parts of γ-ammonia (2,3-propylene oxide) propyltrimethoxysilane, 3 parts of γ-(methacryloyloxy) propyltrimethyl Oxysilane, 10 parts of six-functional polyurethane acrylate 5290 of Changchun Chemical Industry, 5 parts of bifunct...

Embodiment 2

[0044] A method for preparing a UV-curable transfer adhesive for a glass substrate, comprising the following steps:

[0045] In parts by weight, 25 parts of nine-dimensional commercial carboxyl group-containing trifunctional resin UA-787LV, 5 parts of Changchun Chemical's hexafunctional polyurethane acrylate 5290, 13 parts of isobornyl acrylate reactive diluent, 1 part of 2 , 4,6-trimethylbenzoyl-diphenylphosphine oxide, 3 parts of 1-hydroxy-cyclohexyl-phenyl ketone, and 3 parts of 2-hydroxyethyl methacrylate phosphate additives were added and stirred in turn In the dispersing machine, normal pressure, 35°C, dark, dry, ventilated environment, stirred at 1000 rpm for 4 hours, stirred and dispersed evenly, filtered clean impurities, protected from light, sealed and packaged, as the main agent;

[0046] In parts by weight, 8 parts of 2-hydroxyethyl acrylate, 2 parts of γ-ammonia (2,3-propylene oxide) propyltrimethoxysilane, 3 parts of γ-(methacryloyloxy) propyltrimethyl Oxysilan...

Embodiment 3

[0049] A method for preparing a UV-curable transfer adhesive for a glass substrate, comprising the following steps:

[0050] In parts by weight, 30 parts of nine-dimensional commercial trifunctional resin UA-787LV containing carboxyl groups, 13 parts of isobornyl acrylate reactive diluent, 1 part of 2,4,6-trimethylbenzoyl-di Phenylphosphine oxide, 3 parts of 1-hydroxy-cyclohexyl-phenyl ketone, and 3 parts of 2-hydroxyethyl methacrylate phosphate additives were sequentially added into the stirring disperser. In a dry and ventilated environment, stir at 1000 rpm for 4 hours, stir and disperse evenly, filter out impurities, keep away from light, and seal the package as the main ingredient;

[0051] In parts by weight, 2 parts of γ-ammonia (2,3-epoxypropylene) propyltrimethoxysilane, 3 parts of γ-(methacryloxy) propyltrimethoxysilane, 10 parts of Changchun Chemical Industry’s six Functional polyurethane acrylate 5290, 5 parts of 1,6-hexanediol diacrylate, 8 parts of 2-hydroxyethy...

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Abstract

The invention discloses an ultraviolet curing transfer adhesive for a glass substrate. The ultraviolet curing transfer adhesive comprises aliphatic polyurethane acrylate, an acrylate active diluent, a photoinitiator, an acrylate aid and a silane coupling agent. The ultraviolet curing transfer adhesive for a glass substrate, disclosed by the invention, has good mechanical property, wear resistance, solvent resistance and cold / hot impact resistance while the adhesion between the adhesive layer and the substrate is good; and particularly, after water boiling test, the adhesion between the adhesive layer and the substrate is still greater than 4B, and little environmental pollution is caused. The problems that existing ultraviolet curing transfer adhesive has low adhesion and is not resistant to water boiling and solvent are solved; and the ultraviolet curing transfer adhesive disclosed by the invention meets the industry requirements, reduces the production cost of an enterprise and brings profit to the enterprise.

Description

technical field [0001] The invention relates to the technical field of transfer adhesives, in particular to an ultraviolet light-cured transfer adhesive for glass substrates, which can be used on the surface of inorganic materials such as glass, and solves the problem that the existing transfer adhesives can only be applied to organic films. Background technique [0002] UV curing curing transfer adhesive has the advantages of convenient use, fast curing speed, high light transmittance, convenient operation, and environmental friendliness, and has been widely used in various plastic film industries. The formula of UV curing transfer printing adhesive generally includes: reactive diluent monomers, photoinitiators, acrylate prepolymers, additives, etc. [0003] UV curing is ultraviolet curing. UV is the English abbreviation of ultraviolet. Curing refers to the process of transforming a substance from a low molecular weight to a high molecular weight. Under UV radiation, the ph...

Claims

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Application Information

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IPC IPC(8): C09J175/14C09J11/06
Inventor 葛大鹏曾建伟鲁斌高显波
Owner SUZHOU BETELY POLYMER MATERIALS CO LTD
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