Molybdenum sulfide catalyst and preparation thereof, and applications of molybdenum sulfide catalyst in hydrogenation degradation of aromatic phenol and ether compounds
A technology for hydrogenation degradation of ether compounds, applied in the field of catalytic conversion of biomass derivatives, can solve the problems of low yield and high price of aromatic products, and achieve the effects of low price, easy preparation and good application prospects
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Embodiment 1
[0023] MoS2 Preparation of / AC catalyst: Dissolve 0.92g of ammonium heptamolybdate tetrahydrate in 9mL of deionized water, add 4.5g of activated carbon after completely dissolving, impregnate at room temperature for 24h, dry in an oven at 120°C for 12h, and turn the catalyst precursor to Put it into a tube furnace, bake at 450°C for 3h under Ar atmosphere, cool to room temperature, and then perform temperature-programmed vulcanization. The specific vulcanization process is: heat up from room temperature at 5°C / min to 400°C, then keep it for 4h, and cool under Ar atmosphere to room temperature, H 2 S / H 2 The total flow rate is 60mL / min, H 2 S volume fraction of 10% yielded MoS with 10 wt% Mo loading 2 / AC Catalyst.
Embodiment 2
[0025] MoS 2 / γ-Al 2 o 3 Preparation of the catalyst: the preparation process is similar to Example 1, the difference is that the support is replaced by γ-Al 2 o 3 , during calcination, the precursor was transferred to a muffle furnace under an air atmosphere, and then transferred to a tube furnace for temperature-programmed vulcanization to obtain MoS with a Mo loading of 10wt%. 2 / γ-Al 2 o 3 catalyst.
Embodiment 3
[0027] MoS 2 / SiO 2 Preparation of catalyst: the preparation process is similar to Example 2, except that the carrier is replaced by SiO 2 , to obtain MoS with a Mo loading of 10 wt% 2 / SiO 2 catalyst.
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