Thermosetting resin composition and prepreg made of thermosetting resin composition, as well as laminated board
A technology of resin composition and prepreg, applied in synthetic resin layered products, lamination, lamination devices, etc., can solve the problems of poor adhesion, low heat resistance, damage to the dielectric properties of the system, etc.
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Synthetic example 1
[0057] Put N-(4-hydroxyphenyl)maleimide (190g, 1mol), phenol (94g, 1mol, M94) and oxalic acid (10g) into the flask equipped with thermometer, condenser and stirrer, mix and stir After uniformity, put it in a constant temperature water bath at 70°C; then, under stirring, add formaldehyde solution (150mL, the ratio of phenol / aldehyde to 1 / 0.8) dropwise into the flask for 0.5 hours; after adding formaldehyde, maintain 70°C The temperature and stirring conditions were reacted for 15 hours; then, the reaction product was dissolved and diluted with 400mL acetone, and then the reaction product was precipitated with 40% methanol aqueous solution; the above dissolution-precipitation operation was repeated 3 to 5 times, and it was filtered, separated, Drying yielded pure maleimide phenolic formaldehyde (P-1).
[0058] Take 100g of maleimide phenolic novolac (P-1) prepared by the above method and 500g of methyl isobutyl ketone solvent and put them in a flask to fully mix and dissolve, de...
Synthetic example 2
[0061] With reference to the method of synthetic example 1, the maleimide ester (B-2) of following structure is obtained:
[0062] ; Among them, Ar is , R is phenyl;
[0063] Among them, n is 1~10, and the ratio of x to y is 0.5:1.
Synthetic example 3
[0065] With reference to the method for synthetic example 1, the maleimide ester (B-3) of following structure is obtained:
[0066] ; Among them, Ar is: , R is maleimidophenyl;
[0067] Among them, n is 1~10, and the ratio of x to y is 0.1:1.
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