Preparation method of cement grinding aid
A technology of cement grinding aid and triethanolamine, which is applied in the field of cement grinding aid preparation, can solve the problems of cement or concrete hazards and effect differences, and achieve the elimination of ball paste grinding, elimination of electrostatic adsorption, and optimization of cement particle gradation Effect
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Embodiment 1
[0024] A preparation method of cement grinding aid, comprising the following steps:
[0025] (1) Raw material preparation: Weigh the raw materials according to the parts by mass: 10 parts of propylene glycol, 3 parts of unsaturated polyester resin, 6 parts of sodium thiosulfate, 2 parts of calcium formate, 0.6 parts of Tween-80, alkyl polyglycoside 6 parts, 10 parts of maleic anhydride, 2 parts of nano silicon dioxide, 2.4 parts of sodium hexametaphosphate, 2 parts of allyl polyoxyethylene ether, 1.8 parts of water-retaining cellulose;
[0026] (2) Preparation of modified triethanolamine:
[0027] A configures the acid mixed solution of sulfuric acid and phosphoric acid, and the mol ratio of described sulfuric acid and phosphoric acid is 1:1.1;
[0028] B heat the triethanolamine solution to 130-135 ° C, drop the acid mixed solution, the mass ratio of the triethanolamine to the acid mixed solution is 2:1;
[0029] C maintained at 130-135°C and stirred for 3 hours, then coole...
Embodiment 2
[0033] A preparation method of cement grinding aid, comprising the following steps:
[0034] (1) Raw material preparation: Weigh the raw materials according to the parts by mass: 11 parts of propylene glycol, 3.5 parts of unsaturated polyester resin, 7 parts of sodium thiosulfate, 3 parts of calcium formate, 0.65 parts of Tween-80, alkyl polyglycoside 7 parts, 12 parts of maleic anhydride, 2.5 parts of nano silicon dioxide, 3 parts of sodium hexametaphosphate, 3 parts of allyl polyoxyethylene ether, 2.1 parts of water-retaining cellulose;
[0035] (2) Preparation of modified triethanolamine:
[0036] A configures the acid mixed solution of sulfuric acid and phosphoric acid, and the mol ratio of described sulfuric acid and phosphoric acid is 1:1.2;
[0037] B heat the triethanolamine solution to 130-135 ° C, drop the acid mixed solution, the mass ratio of the triethanolamine to the acid mixed solution is 2.2:1;
[0038] C is maintained at 130-140 ° C and stirred for 3 hours, ...
Embodiment 3
[0042] A preparation method of cement grinding aid, comprising the following steps:
[0043] (1) Raw material preparation: Weigh the raw materials according to the parts by mass: 12 parts of propylene glycol, 4 parts of unsaturated polyester resin, 9 parts of sodium thiosulfate, 5 parts of calcium formate, 0.7 parts of Tween-80, alkyl polyglycoside 9 parts, 20 parts of maleic anhydride, 4 parts of nano silicon dioxide, 4 parts of sodium hexametaphosphate, 4 parts of allyl polyoxyethylene ether, 3.2 parts of water-retaining cellulose;
[0044] (2) Preparation of modified triethanolamine:
[0045] A configures the acid mixed solution of sulfuric acid and phosphoric acid, and the mol ratio of described sulfuric acid and phosphoric acid is 1:1.2;
[0046] B heat the triethanolamine solution to 135-140 ° C, drop the acid mixed solution, the mass ratio of the triethanolamine to the acid mixed solution is 2.5:1;
[0047] C is maintained at 130-140 ° C and stirred for 3 hours, then ...
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