Preparation method of flame-retardant composite over-rust antirust paint
A rust-proof, flame-retardant composite technology, used in anti-corrosion coatings, fire-retardant coatings, coatings, etc., can solve the problems of poor uniform compactness and fluidity, weak hydrolysis resistance, and poor adhesion of anti-rust paints. Simple preparation steps, good uniformity and compactness, and strong hydrolysis resistance
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example 1
[0015] First, according to the mass ratio of 1:2, take tung seeds and Maofeng and put them in a 50°C oven to dry for 6 hours, then crush them, pass through a 100-mesh sieve, and then put the sieved particles and lime water into In the container, use a phosphoric acid solution with a mass fraction of 20% to adjust the pH to 7.2, let it stand at 60°C for 10 minutes, then filter and collect the filter residue, put the filter residue in an air dryer to dry; then mix the air-dried filter residue and distilled water according to the mass ratio 1:3, put it into a refiner for refining, place the obtained slurry in an ultrasonic heater, heat it to 70°C in an ultrasonic environment, keep the temperature for 5h, cool it down to 35°C, add distilled water volume 60% n-hexane alkane, keep the temperature for 2h, then filter while it is hot, and collect the filtrate; then in parts by weight, get 30 parts of the above-mentioned filtrate, 10 parts of hectorite, 8 parts of mass fractions of 4.6m...
example 2
[0018] First, according to the mass ratio of 1:2, take tung seeds and Maofeng and put them in a 50°C oven to dry for 7 hours, then crush them, pass through a 100-mesh sieve, and then put the sieved particles and lime water into In the container, adjust the pH to 7.5 with a mass fraction of 20% phosphoric acid solution, let it stand at 65°C for 15 minutes, then filter and collect the filter residue, put the filter residue into an air dryer to dry; then mix the air-dried filter residue and distilled water according to the mass ratio 1:2, put it into a refiner for refining, put the obtained slurry in an ultrasonic heater, heat it to 75°C in an ultrasonic environment, keep the temperature for 6h, cool it down to 38°C, add distilled water volume 63% n-hexane alkane, keep the temperature for 3h, then filter while it is hot, and collect the filtrate; then in parts by weight, get 33 parts of the above-mentioned filtrate, 13 parts of hectorite, 10 parts of mass fraction of 4.6mol / L phos...
example 3
[0021]First, according to the mass ratio of 1:2, take tung seeds and Maofeng and put them in a 50°C oven to dry for 8 hours, then crush them, pass through a 100-mesh sieve, and then put the sieved particles and lime water into In the container, adjust the pH to 7.8 with a phosphoric acid solution with a mass fraction of 20%, let it stand at 70°C for 20 minutes, then filter and collect the filter residue, put the filter residue into an air dryer to dry; then mix the air-dried filter residue and distilled water according to the mass ratio 1:2, put it into a refiner for refining, place the obtained slurry in an ultrasonic heater, heat it to 80°C in an ultrasonic environment, keep the temperature for 8 hours, cool down to 40°C, add distilled water volume 65% n-hexane alkane, keep the temperature for 3h, then filter while it is hot, and collect the filtrate; then in parts by weight, get 35 parts of the above-mentioned filtrate, 15 parts of hectorite, 11 parts of mass fraction of 4.6...
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