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Graphene/nano-silver light-sensitive conductive composite paste and preparation method therefor

A technology of composite slurry and graphene, which is applied in cable/conductor manufacturing, conductive materials dispersed in non-conductive inorganic materials, nanotechnology, etc., can solve the problems of low conductivity, insufficient strength and complicated process, etc., and achieve development Clean and clear, clear graphics, good particle size effect

Inactive Publication Date: 2016-08-17
SHENZHEN GUOCHUANG JIAWEI GRAPHENE TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] In the above technical solution, the strength and conductivity of the composite paste can be improved through the combination of graphene and silver, but the process is complicated, and the conductivity and strength are not high enough

Method used

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  • Graphene/nano-silver light-sensitive conductive composite paste and preparation method therefor
  • Graphene/nano-silver light-sensitive conductive composite paste and preparation method therefor
  • Graphene/nano-silver light-sensitive conductive composite paste and preparation method therefor

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037]In parts by weight, photosensitive resin 20, novolak epoxy resin (F-51) 5, graphene 15, spherical nano-silver powder (NAg-20D) 50, photoinitiator (907) 3, dispersant (polyurethane AFCONA- 4010) 4. Defoamer (organic silicon AFCONA-2501) 2. Propylene glycol methyl ether acetate 50, divalent ester 80

[0038] 1) Take 15 parts by mass of graphene and dry it in a vacuum drying oven (baking at 100°C for 4h) to remove moisture;

[0039] 2) Under the condition of yellow light, mix photosensitive resin 20, thermosetting resin (F-51) 5, graphene 15, nano-silver powder 50, dibasic acid ester 80, dispersant (AFCONA-4010) 4 Mix and add to a mixer, control the rotation speed at 1000 rpm, and stir for 2 hours to obtain the first mixture;

[0040] 3) Add the first mixture to a nano sand mill for graded grinding and dispersion under yellow light conditions; specifically, grind and disperse for 4 hours under the condition of zirconium beads with a particle size of 1.0 mm; then grind and ...

Embodiment 2

[0043] In parts by weight, photosensitive resin 40, novolac epoxy resin (F-51) 8, graphene 20, nano silver powder (NAg-20D) 50, photoinitiator (TPO) 3, dispersant (polyurethane AFCONA-4010 ) 4. Defoamer (organic silicon AFCONA-2501) 2. Propylene glycol methyl ether acetate 50, divalent ester 100

[0044] 1) Take 20 parts by mass of graphene and dry it in a vacuum drying oven (baking at 100°C for 4 hours) to remove moisture;

[0045] 2) Under the condition of yellow light, mix photosensitive resin 40, thermosetting resin (F-51) 8, graphene 20, nano-silver powder 60, divalent ester 1000, dispersant (AFCONA-4010) 4 according to the above mass parts Mixed and added to the mixer, the control speed is 1000rpm, and the stirring time is 2h;

[0046] 3) Add the first mixture to the nano sand mill under yellow light conditions for graded grinding and dispersion (zirconium beads with a particle size of 1.0 mm are ground and dispersed for 4 hours, and zirconium beads with a particle size...

Embodiment 3

[0049] In parts by weight, photosensitive resin 30, novolac epoxy resin (F-51) 10, graphene 20, nano silver powder (NAg-20D) 50, photoinitiator (907) 3, dispersant (polyurethane AFCONA-4010 ) 4. Defoamer (organic silicon AFCONA-2501) 2. Propylene glycol methyl ether acetate 50, divalent ester 100

[0050] 1) Take 20 parts by mass of graphene and dry it in a vacuum drying oven (baking at 100°C for 4 hours) to remove moisture;

[0051] 2) Under the condition of yellow light, according to the above mass parts, mix photosensitive resin 30, thermosetting resin (F-51) 5, graphene 20, nano-silver powder 60, divalent ester 80, dispersant (AFCONA-4010) 4 Mix and add to a mixer, control the rotation speed at 1000 rpm, and stir for 2 hours to obtain the first mixture;

[0052] 3) Add the first mixture to the nano sand mill under yellow light conditions for graded grinding and dispersion (zirconium beads with a particle size of 1.0 mm are ground and dispersed for 4 hours, and zirconium b...

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Abstract

The invention discloses graphene / nano-silver light-sensitive conductive composite paste and a preparation method therefor. The composite paste comprises the following raw materials based on weight: graphene and spherical nano-silver, wherein the weight ratio of graphene to spherical nano-silver is 1 to 2.0-3.5; and the preparation process comprises the steps of drying graphene and then mixing the raw materials under yellow light to obtain the composite paste. Due to the reasonable formula of the graphene and nano-silver and the new technological method, the light-sensitive silver paste obtains the characteristics of clear image development, high resolution, extremely high conductivity, high coating film strength and the like; the paste is subjected to silk-screen printing, letterpress printing, surface drying, exposing and developing to obtain a pattern with the required high resolution (L / S is greater than 30 / 30[mu]m); and in addition, the composite paste has excellent printing performance, high storage stability, excellent conductivity, high resolution, and high adhesive force.

Description

technical field [0001] The photosensitive and conductive composite material of the present invention is, in particular, a graphene / nano-silver photosensitive composite paste. [0002] The invention also relates to a preparation method, that is, a preparation method of the graphene / nano-silver photosensitive and conductive composite slurry. Background technique [0003] With the rapid development of the touch and display industry, people have higher and higher quality requirements for touch and display equipment (electronic communication touch and display equipment, multimedia and public information query display equipment, industrial control display equipment, etc.). On the one hand, it is required to achieve precise positioning, rapid sensing, and multi-touch in terms of functions. On the other hand, it can achieve features such as thinness and lightness in appearance. Large screens, high image quality, and high resolution have become various touch and display devices. The...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01B1/22H01B1/24H01B13/00B82Y30/00B82Y40/00
CPCH01B1/22B82Y30/00B82Y40/00H01B1/24H01B13/00
Inventor 姜宗清郭焕焕钟起权
Owner SHENZHEN GUOCHUANG JIAWEI GRAPHENE TECH CO LTD
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