Preparation method of high-purity spherical nano molybdenum disulfide
A nano-molybdenum disulfide, spherical technology, applied in the direction of molybdenum sulfide, nanotechnology, nanotechnology, etc., can solve the problem of uneven surface of molybdenum disulfide spheres, and achieve the effects of uniform size, simple reaction process and regular morphology.
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Embodiment 1
[0033] The mixed solution (V 无水乙醇 / V 去离子水 =1 / 19), add 2 mL of hydrazine hydrate after stirring evenly, transfer the solution into a high-pressure reactor with a volume of 100 mL after mixing evenly, seal it and place it in a 200°C incubator, keep it warm for 24 hours, cool to room temperature, and use After washing with deionized water and absolute ethanol, place it in a vacuum oven at 70°C for 8 hours to obtain the high-purity spherical nanomolybdenum disulfide required in this case.
[0034] Depend on figure 1 It can be seen that the product is composed of nanospheres with a particle size of about 400nm, the particle size distribution range of the spheres is narrow, the spherical structure is complete, and the dispersibility of the spheres is good.
[0035] Depend on figure 2 The XRD shows that the structure of molybdenum disulfide is 2H-MoS 2 .
Embodiment 2
[0037] The mixed solution (V 无水乙醇 / V 去离子水 =3 / 17), after stirring evenly, add 2mL of hydrazine hydrate, after mixing evenly, move the solution into a 100mL autoclave, seal it and place it in a 200°C incubator, keep it warm for 24h, cool to room temperature, and use After washing with deionized water and absolute ethanol, place it in a vacuum oven at 70°C for 8 hours to obtain the high-purity spherical nanomolybdenum disulfide required in this case. For the experimental results, see image 3 .
Embodiment 3
[0039] The mixed solution (V 无水乙醇 / V 去离子水 =1 / 3), after stirring evenly, add 2mL of hydrazine hydrate, after mixing evenly, transfer the solution into a 100mL autoclave, seal it and place it in a 180°C incubator, keep it warm for 12h, cool to room temperature, and use After washing with deionized water and absolute ethanol, place it in a vacuum oven at 70°C for 8 hours to obtain the spherical nanomolybdenum disulfide required in this case. For the experimental results, see Figure 4 .
[0040] According to the SEM image, the spherical structure of the prepared nanomolybdenum disulfide is complete, and the size distribution is narrow at about 400nm.
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