Cadmium sulfide target material preparing method and device
A preparation device and cadmium sulfide technology, which is applied in the field of cadmium sulfide target preparation, can solve the problems of many intermediate links and operation steps, the reduction of the purity of cadmium sulfide target material, and the toxicity of cadmium sulfide dust, so as to achieve less intermediate links and operation steps , It is conducive to large-scale production and the effect of improving the purity of the target material
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[0034] The invention provides a method for preparing a cadmium sulfide target material, comprising the following steps: loading cadmium sulfide powder into a mold for pre-pressing to obtain pre-pressed cadmium sulfide powder; Put it into a hot-press sintering furnace, and hot-press and vacuum sinter to obtain a cadmium sulfide target.
[0035] Use a hot isostatic graphite mold to pre-press the cadmium sulfide powder with a purity of 4-5N and a powder particle size of 1 micron to 200 microns, and combine one or more layers of pre-pressed cadmium sulfide powder together with the graphite mold Put them together into a hot-press sintering furnace. If it is multi-layer pre-pressed cadmium sulfide powder, graphite gaskets are required to separate the cadmium sulfide powder. Pump the vacuum down to below 5Pa; heat the cadmium sulfide powder after pre-pressing in the furnace body, first raise the temperature to 350-550°C at a rate of 8-12°C / min, and keep it warm for 30-60min; Raise t...
Embodiment 1
[0038] Weigh 1350g of 5N cadmium sulfide with a particle size of 200 microns and put it into a graphite mold with a size of 166*166mm. Pump the vacuum to below 600Pa, and then turn on the Roots pump to evacuate until the vacuum degree is less than 5Pa. Turn on the temperature control system, so that the temperature in the furnace starts to rise to 350°C at a rate of 8°C / min, and hold for 30 minutes, then continue to heat up to 650°C at a rate of 5°C / min, and start holding for 30 minutes. The hydraulic station provides vertical pressure to the graphite mold in the furnace through the movement of the pressure head. The pressure increase rate is 3T / min. When the pressure slowly increases to 85T, stop the pressure increase, close the hydraulic station, continue to keep warm at 650°C for 45min and keep the pressure constant At 85T, after the heat preservation is over, the furnace body begins to cool down naturally. When the temperature drops below 500°C, start to slowly reduce the ...
Embodiment 2
[0040]Weigh two parts of 1450g of 4N cadmium sulfide with a particle size of 100 microns, and put one part into the bottom layer of the graphite mold that has been wiped clean. The size of the mold is 175*140mm. Gasket, and then put the second weighed cadmium sulfide raw material on the graphite gasket, cold pre-press molding again, put the graphite mold into the hot-press sintering furnace, close the furnace door, and first extract the cadmium sulfide through the slide valve vacuum pump Vacuum to below 600Pa, and then turn on the Roots pump to evacuate until the vacuum degree is less than 5Pa. Turn on the temperature control system, so that the temperature in the furnace starts to rise to 400°C at a rate of 10°C / min, and hold for 40 minutes, then continue to heat up to 750°C at a rate of 7°C / min, and start to hold for 40 minutes, and turn on the hot-press sintering furnace. The hydraulic station provides vertical pressure to the graphite mold through the downward movement of ...
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