Quick drying type color fixing agent and preparation method thereof
A color-fixing agent and quick-drying technology, applied in dyeing, textile and papermaking, etc., can solve the problems of long interval time and low efficiency of preparation process, and achieve the effect of easy operation, simple preparation process and shortening of the overall process.
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Embodiment 1
[0017] S1: Stir 15 parts of 2,5-dichlorobenzoic acid, 8 parts of pinacolone, 8 parts of 4,2-dinitroanisole and 10 parts of cyclohexanol at room temperature for 15 minutes;
[0018] S2: Stir 10 parts of sorbic acid, 18 parts of anthranil, 7 parts of triethylenetetramine and 50 parts of distilled water at a temperature of 30° C. for 20 minutes;
[0019] S3: Mix 6 parts of 2-amino-3,4-dihydroxybenzophenone and 3 parts of α,α-diethoxyacetophenone and add to step S2, stir for 5 minutes and then add the mixed solution in step S1, Stir again for 10 minutes, then raise the temperature to 70°C, let stand for 8 minutes, and then stir again for 20 minutes; the fast-drying color fixing agent can be obtained after the solution is cooled.
Embodiment 2
[0025] S1: Stir 25 parts of 2,5-dichlorobenzoic acid, 13 parts of pinacolone, 15 parts of 4,2-dinitroanisole and 18 parts of cyclohexanol at room temperature for 20 minutes;
[0026] S2: Stir 20 parts of sorbic acid, 26 parts of anthranil, 13 parts of triethylenetetramine and 80 parts of distilled water at a temperature of 40° C. for 30 minutes;
[0027] S3: Mix 12 parts of 2-amino-3,4-dihydroxybenzophenone and 15 parts of α,α-diethoxyacetophenone and add to step S2, stir for 5 minutes and then add the mixed solution in step S1, Stir again for 15 minutes, then raise the temperature to 80°C, let stand for 10 minutes, and then stir again for 30 minutes; the fast-drying color fixing agent can be obtained after the solution is cooled.
Embodiment 3
[0033] S1: Stir 18 parts of 2,5-dichlorobenzoic acid, 10 parts of pinacolone, 10 parts of 4,2-dinitroanisole and 12 parts of cyclohexanol at room temperature for 15 minutes;
[0034] S2: Stir 13 parts of sorbic acid, 20 parts of anthranil, 9 parts of triethylenetetramine and 65 parts of distilled water at a temperature of 30° C. for 20 minutes;
[0035] S3: Mix 8 parts of 2-amino-3,4-dihydroxybenzophenone and 5 parts of α,α-diethoxyacetophenone and add to step S2, stir for 5 minutes and then add the mixed solution in step S1, Stir again for 10 minutes, then raise the temperature to 70°C, let stand for 8 minutes, and then stir again for 20 minutes; the fast-drying color fixing agent can be obtained after the solution is cooled.
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