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Thermal repair material for carbon-free refined ladle base brick and preparation method thereof

A hot-state repairing and repairing material technology, applied in the field of hot-state repairing materials and its preparation, can solve problems such as differences in repairing material index requirements, poor sintering performance of repairing materials, and difficulty in ensuring construction quality, and achieve flexible construction methods and excellent preparation methods. Simple and easy to use, excellent performance

Active Publication Date: 2020-05-22
SHANGHAI BAOSTEEL IND TECHNOLOGICAL SERVICE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Chinese patent application "Replenishment method of ladle breathable brick" (CN101985672 A) introduces the technology of repairing breathable brick under high temperature, which adds a certain amount of sintered materials such as fiber and clay on the basis of the original breathable brick material, but it does not involve Block repair
[0006] The Chinese patent "A Hot Repair Method for Ladle Ventilation Bricks" (CN101844224B) introduces a method of repairing the depressions with a repairing material in the case of depressions in the ventilation bricks. It can be used for refining ladles and non-refining ladles, but for repair There are differences in the requirements of material indicators, and it does not involve the repair of seat bricks
[0008] However, the development of ventilation brick and seat brick repair technology is still not perfect so far. There is a lot of room for research and development in both repair technology and repair materials. The main problems at present are poor sintering performance and low bonding strength of repair materials. , construction quality is difficult to guarantee, etc.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] With 50~60wt% high alumina bauxite aggregate, 20~30wt% corundum fine powder, 4~10wt% grade 70 spinel fine powder, 4~10wt% magnesia fine powder, 0.5~ 4 wt % SiO 2 Micronized powder, 1~5 wt % α-Al 2 o 3 Micropowder and 1~5 wt% aluminate cement are used as raw materials, plus 0.1~0.2 wt% polycarboxylate water reducer and 1~2.0 wt% polyphosphate in the weight percentage of raw materials, and fully stirred in the mixer Evenly, a carbon-free refined ladle base brick hot-state repair material is prepared.

[0031]The main physical properties of the hot repair material prepared in this example are: the bond strength after drying at 110°C is 1.0~2.0MPa, the bond strength after 1100°C medium temperature insulation for 1~3 hours is 2.0~4.0MPa, and the bond strength at 1600°C The bond strength after heat preservation at high temperature for 1~3 hours is >8MPa, and the bond strength after thermal shock (1100°C water cooling) three times is 0.5~1.5MPa.

Embodiment 2

[0033] With 60~65wt% high alumina bauxite aggregate, 15~20wt% corundum fine powder, 4~10wt% 78 grade spinel fine powder, 4~10wt% magnesia fine powder, 0.5~ 4 wt % SiO 2 Micronized powder, 1~5 wt % α-Al 2 o 3 Micropowder and 1~5 wt% aluminum dihydrogen phosphate as raw materials, plus 0.1~0.2 wt% polycarboxylate water reducer and 1~2wt% sodium borate in the weight percentage of raw materials, fully stirred in the mixer, A carbon-free refined ladle base brick hot-state repair material is obtained.

[0034] The main physical properties of the hot repair material prepared in this example are: the bond strength after drying at 110°C is 1.0~2.0MPa, the bond strength after 1100°C medium temperature insulation for 1~3 hours is 2.0~4.0MPa, and the bond strength at 1600°C The bond strength after heat preservation at high temperature for 1~3 hours is >8MPa, and the bond strength after thermal shock (1100°C water cooling) three times is 0.5~1.5MPa.

Embodiment 3

[0036] With 65~75 wt % high alumina bauxite aggregate, 10~15 wt % corundum fine powder, 4~10 wt % 90 grade spinel fine powder, 4~10 wt % magnesia fine powder, 0.5 ~4 wt % SiO 2 Micronized powder, 1~5 wt % α-Al 2 o 3 Micropowder and 1-5 wt % aluminum sulfate are used as raw materials, plus 0.1-0.2 wt % polycarboxylate water reducing agent and 1-2 wt % boron glass powder in the weight percentage of the raw materials, fully stirred in the mixer, A carbon-free refined ladle base brick hot-state repair material is obtained.

[0037] The main physical properties of the hot repair material prepared in this example are: the bond strength after drying at 110°C is 1.0~2.0MPa, the bond strength after 1100°C medium temperature insulation for 1~3 hours is 2.0~4.0MPa, and the bond strength at 1600°C The bond strength after heat preservation at high temperature for 1~3 hours is >8MPa, and the bond strength after thermal shock (1100°C water cooling) three times is 0.5~1.5MPa.

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PUM

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Abstract

The present invention discloses a carbon-free refined steel ladle base brick thermal-state repair material and a preparation method thereof. The repair material comprises 50-75 wt% of bauxite aggregate or corundum aggregate, 10-30 wt% of corundum fine powder, 4-10 wt% of magnesia fine powder, 4-10 wt% of spinel fine powder, 0.5-4 wt% of SiO2 micro-powder, 1-5 wt% of alpha-Al2O3 micro-powder, and 1-5 wt% of a binder. According to the production method, the repair material is adopted as a raw material, a water reducing agent accounting for 0.1-0.2 wt% of the repair material and a sintering agent accounting for 1-2 wt% of the repair material are added, the obtained mixture is placed into a stirrer, and complete and uniform stirring is performed to obtain the carbon-free refined steel ladle base brick thermal-state repair material. According to the present invention, the defects of the traditional base brick repair material are overcome; the preparation method is simple and easy to perform; the dry construction can be achieved, and the water can be added on the site to form the self-flowing material so as to construct; the construction is simple, safe and environment-friendly, and the quick base brick repair can be achieved; and the material has characteristics of low cost, excellent use performance, and flexible construction method.

Description

technical field [0001] The invention relates to a hot-state repair material for carbon-free refined ladle base bricks and a preparation method thereof. Background technique [0002] In the iron and steel metallurgy industry, the ladle was originally just a transmission device on the molten steel continuous casting operation line. In recent years, with the development of out-of-furnace refining and continuous casting technology, the use of ladles for secondary refining has become the mainstream process in major steel mills. The air-permeable bricks at the bottom of the ladle and the supporting bricks are the key components to achieve the purpose of secondary refining. [0003] After the molten steel enters the ladle, the molten steel is stirred by blowing argon gas into the molten steel through the use of breathable bricks, so as to quickly realize the homogenization of the temperature and chemical composition of the molten steel in the metallurgical process, remove the inclu...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/66
Inventor 邱文冬韩兵强崔秀君柯昌明何晓俊刘延山李楠
Owner SHANGHAI BAOSTEEL IND TECHNOLOGICAL SERVICE
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