Preparation method for ceramic binder used for rapid synthesis of CBN abrasive tools by microwave method
A technology of vitrified bond and synthesis method, which is applied in the field of rapid synthesis of vitrified bond for CBN abrasive tools by microwave method, which can solve the problems of poor fatigue resistance, high sintering temperature, and low strength of vitrified bond, and achieve bending resistance The effect of high strength, low reaction temperature and short reaction time
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Embodiment 1
[0024] Take by weight 34.8g of silicon dioxide, 9.36g of aluminum hydroxide, 12.4g of sodium oxide and 19.8g of boric acid of analytical grade, after fully mixing, pass through a 200 mesh sieve, and then raise the mixture to 1500 at a certain heating rate. ℃, and keep warm for 2~5h. After water cooling, drying, crushing and ball milling, the basic vitrified bond is obtained. After pressing, drying, microwave firing and other processes, the refractoriness and flexural strength of the binder were measured respectively. The results show that the refractoriness of the binder is 500~600℃, and the flexural strength is 55~110MPa.
Embodiment 2
[0026] Weigh 61.8g of silicic acid, 11.5g of aluminum hydroxide, 17.0g of anhydrous sodium carbonate and 27.5g of diboron trioxide of analytical grade by weight. Raise to 1400°C and keep warm for 2~5h. After water cooling, drying, crushing and ball milling, the basic vitrified bond is obtained. After pressing, drying, microwave firing and other processes, the refractoriness and flexural strength of the binder were measured respectively. The results show that the refractoriness of the binder is 500~600℃, and the flexural strength is 55~110MPa.
Embodiment 3
[0028] Take by weight 53.65g of silicon dioxide, 7.66g of aluminum oxide, 12.25g of sodium oxide and 20.86g of boric acid of analytical purity, after fully mixing, pass through a 200 mesh sieve, and then the mixture is raised to 1300°C, and keep it warm for 2~5h. After water cooling, drying, crushing and ball milling, the basic vitrified bond is obtained. After pressing, drying, microwave firing and other processes, the refractoriness and flexural strength of the binder were measured respectively. The results show that the refractoriness of the binder is 500~600℃, and the flexural strength is 55~110MPa.
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