A kind of bright, warm, lightweight fiber and preparation method thereof
A light and bright technology, applied in fiber processing, filament/thread forming, chemical post-treatment of synthetic polymer artificial filament, etc., can solve problems such as easy generation of static electricity, hair, loops, and increased difficulty in quality control, and achieve Effect of light weight, improved smoothness, and increased air permeability
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Embodiment 1
[0052] A method for preparing bright, warm and lightweight fibers. Firstly, an oiling oil is prepared. The specific preparation steps are as follows: blend the initiator butanol and strong alkali potassium hydroxide, then raise the temperature to 105°C, and then add and mix evenly The amount of ethylene oxide, [(1,1,2,2-tetrafluoroethoxy) methyl] ethylene oxide and propylene oxide, the amount of butanol is ethylene oxide, [(1,1, 2,2-tetrafluoroethoxy) methyl] 1‰ of the total mass of ethylene oxide and propylene oxide, the amount of strong base potassium hydroxide is ethylene oxide, [(1,1,2,2- 1‰ of the total mass of tetrafluoroethoxy)methyl]oxirane and propylene oxide, ethylene oxide, [(1,1,2,2-tetrafluoroethoxy)methyl]oxirane The molar ratio of alkanes and propylene oxide is 10:1:20, the polymerization reaction is carried out under the protective atmosphere of nitrogen atmosphere, the reaction pressure is 0.4MPa, and after the relative molecular weight is 1000, the fluorine-c...
Embodiment 2
[0066] A method for preparing bright, warm and lightweight fibers. Firstly, an oiling oil is prepared. The specific steps are: blend the initiator butanol and strong alkali sodium hydroxide, then raise the temperature to 125°C, and then add the evenly mixed ring Ethylene oxide, [(1,1,2,2-tetrafluoroethoxy)methyl]oxirane and propylene oxide, the amount of butanol is ethylene oxide, [(1,1,2, 2-tetrafluoroethoxy) methyl] 5‰ of the total mass of ethylene oxide and propylene oxide, the amount of strong alkali sodium hydroxide is ethylene oxide, [(1,1,2,2-tetrafluoro 5‰ of the total mass of ethoxy)methyl]oxirane and propylene oxide, ethylene oxide, [(1,1,2,2-tetrafluoroethoxy)methyl]oxirane and The amount of propylene oxide is 20:3:30 in molar ratio, the polymerization reaction is carried out under the protective atmosphere of inert gas atmosphere, the reaction pressure is 0.5MPa, and after the relative molecular weight is 4000, neutralization, adsorption, vacuum dehydration and dry...
Embodiment 3
[0080] A method for preparing bright, warm and lightweight fibers. Firstly, an oiling oil is prepared. The specific steps are as follows: blend the initiator butanol and strong alkali sodium hydroxide, then raise the temperature to 115°C, and then add evenly mixed ring Ethylene oxide, [(1,1,2,2-tetrafluoroethoxy)methyl]oxirane and propylene oxide, the amount of butanol is ethylene oxide, [(1,1,2, 2-tetrafluoroethoxy) methyl] 2‰ of the total mass of ethylene oxide and propylene oxide, the amount of strong alkali sodium hydroxide is ethylene oxide, [(1,1,2,2-tetrafluoro Ethoxy) methyl] 1.5‰ of the total mass of ethylene oxide and propylene oxide, ethylene oxide, [(1,1,2,2-tetrafluoroethoxy) methyl] oxirane and The amount of propylene oxide is 12:1:30 by molar ratio, the polymerization reaction is carried out under the protective atmosphere of an inert gas atmosphere, the reaction pressure is 0.8MPa, and after reaching a relative molecular weight of 3000, neutralization, adsorpti...
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