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Detection method for capsule capable of strengthening body resistance against hepatitis B

A detection method, a technology for righting the body of hepatitis B, applied in measuring devices, instruments, scientific instruments, etc., can solve the problems of unexplained fallback and identification of pig feces and beans, and achieve the effect of safeguarding the interests of patients, simple operation, and ensuring clinical efficacy.

Active Publication Date: 2015-07-22
九寨沟天然药业股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In the existing detection methods for Bgan Fuzheng Capsules, Boluohui and Zhushidou were not identified

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0065] (1) TLC qualitative identification

[0066] TLC qualitative identification of Radix Polygoni Multiflori: Take 10 capsules of this product, take its contents, put it in a conical flask, add 20ml of methanol, shake, ultrasonically extract for 40min, filter, evaporate the filtrate to dryness, add 1ml of methanol to dissolve the residue, As the test solution; take Polygonum multiflorum reference medicinal material 2g in addition, make the contrast medicinal material solution according to the preparation method of the test solution; according to the thin-layer chromatography "Chinese Pharmacopoeia" 2010 edition one appendix VIB test, absorb the above-mentioned test solution 10 μl each of the solution and the control medicinal material solution were spotted on the same silica gel G thin-layer plate, and the chloroform-methanol-water mixture (22:10:1) was used as the developer, developed, taken out, dried, and inspected under a 365nm ultraviolet lamp ; In the chromatogram of t...

Embodiment 2

[0077] (1) TLC qualitative identification

[0078] TLC qualitative identification of Radix Polygoni Multiflori: Take 10 capsules of this product, take its contents, put it in a conical flask, add 40ml of methanol, shake, ultrasonically extract for 25min, filter, evaporate the filtrate to dryness, add 3ml of methanol to dissolve the residue, As the test solution; take Polygonum multiflorum reference medicinal material 2g in addition, make the contrast medicinal material solution according to the preparation method of the test solution; according to the thin-layer chromatography "Chinese Pharmacopoeia" 2010 edition one appendix VIB test, absorb the above-mentioned test solution 5 μl each of the solution and the control medicinal material solution were spotted on the same silica gel G thin-layer plate, and the chloroform-methanol-water mixture (19:8:1) was used as the developer, developed, taken out, dried, and inspected under a 365nm ultraviolet lamp ; In the chromatogram of the...

Embodiment 3

[0089] (1) TLC qualitative identification

[0090] TLC qualitative identification of Radix Polygoni Multiflori: Take 10 capsules of this product, take its contents, put it in a conical flask, add 30ml of methanol, shake, ultrasonically extract for 30min, filter, evaporate the filtrate to dryness, add 2ml of methanol to dissolve the residue, As the test solution; another 2 g of Polygonum multiflorum reference medicinal material is taken, and the contrast medicinal material solution is made according to the preparation method of the test solution; 8 μl each of the product solution and the control medicinal material solution were spotted on the same silica gel G thin-layer plate, and the chloroform-methanol-water mixture (20:9:1) was used as the developer, developed, taken out, dried, and exposed to a 365nm ultraviolet lamp. In the chromatogram of the test product, at the position corresponding to the chromatogram of the control medicinal material, spots of the same color appear;...

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Abstract

The invention discloses a detection method for a capsule capable of strengthening body resistance against hepatitis B. The detection method comprises a thin-layer chromatography qualitative identification item and a content determination item, wherein the thin-layer chromatography qualitative identification item comprises identification of polygonum multiflorum, identification of polygonum cuspidatum and macleaya cordata, identification of cyrtomium fortune, and identification of flatstem milkvetch seed and crotalaria mucronata in the preparation; the content determination item comprises determining the content of salvianolic acid B which is a characteristic ingredient of salvia miltiorrhiza in the preparation. The detection method disclosed by the invention effectively controls the mixture of macleaya cordata and crotalaria mucronata in the capsule capable of strengthening body resistance against hepatitis B, meanwhile effectively controls the ingredients and the content of the capsule capable of strengthening body resistance against hepatitis B, and enables the medicine to be safer and more effective.

Description

technical field [0001] The invention relates to a detection method of medicines, in particular to a detection method of Hepatitis B Fuzheng Capsules. Background technique [0002] Hepatitis B Fuzheng Capsule is a variety recorded in the first volume of traditional Chinese medicine preparations in the "Drug Standards of the Ministry of Health". Its standard number is WS3-B-0001-89. , Danshen, Shayuanzi, ginseng, and ephedra are capsules made of pure Chinese medicine, which have the effects of nourishing the liver and kidney, nourishing qi and activating blood. It is clinically used to treat hepatitis B, and the syndrome differentiation belongs to the syndrome of deficiency of liver and kidney. Clinical manifestations: dull pain and discomfort in the liver area, general fatigue, soreness of the waist and knees, shortness of breath and palpitations, spontaneous sweating, dizziness, anorexia, pale tongue and weak pulse. The drug standard was the earliest drug standard formulat...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/90G01N30/02G01N30/06
Inventor 钟茂团黎黎温国梁杨辉邹波
Owner 九寨沟天然药业股份有限公司
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