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Extraction combination of biologically active substances and ultrasonic microwave combined extraction method

A technology for biologically active substances and combinations, which is applied in the field of biologically active substances extraction, can solve the problem that small volumes of tailings cannot be processed, and achieve the effects of improving or reducing processing capacity, less space, and high degree of intensification.

Active Publication Date: 2016-04-06
YUNNAN KANGZHOU BIOLOGICAL SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0011] Publication No. CN100479898C Chinese patent document discloses a three-frequency ultrasonic extraction device and its method of use. Ultrasonic probes of different frequencies are fixed in the hexahedral vibrator in the center of the extraction tank, so that although ultrasonic vibrations of different frequencies can be produced, different The frequency of ultrasonic vibration will also offset part of the ability of the ultrasonic vibration plate
In addition, the ultrasonic device is required to be immersed in the material liquid, such a fixed volume mode cannot handle small-volume tailings

Method used

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  • Extraction combination of biologically active substances and ultrasonic microwave combined extraction method
  • Extraction combination of biologically active substances and ultrasonic microwave combined extraction method
  • Extraction combination of biologically active substances and ultrasonic microwave combined extraction method

Examples

Experimental program
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Effect test

Embodiment 1

[0039] The structure of the ultrasonic extraction unit see figure 1 : The left and right ultrasonic vibrating plates 1 and the front and rear wall plates (not seen in the figure) form a vertical material chamber, which is divided into eight parts by a central longitudinal baffle 2 and three transverse baffles 3 therein. an extraction chamber. On the corresponding positions of the longitudinal partition 2 and the transverse partition 3, there are material flow holes that allow the material to flow through each extraction chamber from top to bottom (the arrows in the figure indicate the direction of material flow). The feed pipe 4 is connected with an extraction chamber at the top. The nozzle 5 rises to the discharge pipe 6 at the upper part of the material chamber, which is connected with an extraction chamber at the bottom. The ultrasonic vibrating plate 1 is provided with an ultrasonic head 7 at a corresponding position of each extraction chamber. figure 1 Middle 8 is an u...

Embodiment 2

[0047] Carry out the extraction of kidney bean bean powder active substance by the device of embodiment 1. Add water to the first material storage mixing tank, turn on the heating system to heat the interlayer and the liquid in the tank, then add soybean powder as required, and turn on the stirring device for mixing. After the material mixing is completed, the valve can be opened to allow the material liquid to enter the extraction assembly for circular extraction, and filter after the extraction is completed. The filtrate enters the storage tank of the second material storage mixing tank through the conduit. At this time, the extraction of one tank of material is completed, and the first material storage mixing tank is emptied, and materials can be added for the next extraction.

Embodiment 3

[0049] Carry out the extraction of kidney bean bean powder active substance by the device of embodiment 1. Kidney bean bean flour active substance extraction. Add water to the first material storage mixing tank, turn on the heating system to heat the interlayer and the liquid in the tank, then add soybean powder as required, and turn on the stirring device for mixing. After the mixing is completed, the valve can be opened to allow the material liquid to enter the extraction assembly for cyclic extraction, turn on the power supply of the ultrasonic extraction unit and the ultrasonic part in the ultrasonic-microwave extraction unit, and turn off the microwave power supply. At this time, simple ultrasonic treatment is used, but the two The ultrasound frequency is different in the extraction unit. Filtered after sonication at different frequencies and complete extraction. The filtrate enters the emptied secondary material storage mixing tank through the conduit. The first mater...

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Abstract

The invention discloses an extracting assembly for bioactive substances and an ultrasonic-microwave combined extracting method, and belongs to the bioactive substance extracting technology. The extracting assembly is formed by connecting two or three of an ultrasonic-microwave extracting unit, an ultrasonic extracting unit and a microwave extracting unit in series. The extracting assembly is high in integration degree, small in occupied space and capable of realizing ultrasonic-microwave modularization, the microwave head and the ultrasonic head are separated in space, so that mutual interferences between the ultrasonic and the microwaves are reduced, and work can be simultaneously or independently performed according to the material properties; on the condition that the quantity or power of the microwave heads is not increased, the complete processing of an extracting feed liquid by microwaves is achieved without a dead corner, so that a few materials can be processed, and a large number of materials can be processed; a microwave processing mode in the prior art is changed into a short-time mobile continuous processing mode, so that bioactive substances sensitive to heat can be effectively protected.

Description

technical field [0001] The invention belongs to the extraction technology of biological active substances. Background technique [0002] In the extraction of biologically active substances, a large number of studies have shown that ultrasonic extraction and microwave extraction have many advantages. [0003] Ultrasound has: ① mechanical effect. The mechanical action of ultrasound can facilitate the emulsification of liquids, the liquefaction of gels and the dispersion of solids. ② Cavitation. When ultrasonic waves act on liquids, a large number of small air bubbles can be generated. One reason is that there is a local tensile stress in the liquid to form a negative pressure, and the reduction of the pressure makes the gas originally dissolved in the liquid supersaturated, and escapes from the liquid to become small bubbles; the other reason is that the strong tensile stress "tears the liquid apart". " into a hole, called cavitation. Inside the cavity is a liquid vapor o...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D11/02B01J19/10B01J19/12
Inventor 王敏康张跃
Owner YUNNAN KANGZHOU BIOLOGICAL SCI & TECH
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