Compositions comprising solid particles encapsulated in a cross-linked silicone matrix, and methods of making the same
A technology of cross-linking silicone and composition, applied in medical preparations containing active ingredients, skin care preparations, pharmaceutical formulations, etc.
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[0056] TiO 2 Particles were coated first with Gantrez S-97BF polymer and then with KF9909 silicone fluid under sonication, then the coated particles were mixed with more KF9909 silicone fluid in a main beaker and processed using Caframo in Ontario, Canada. Manufactured pro mixer (Model # BDC 1850) at a digital readout of 105 and mix together until a homogeneous mixture is formed. Stannous octoate, commercially available from Arkema as Fascat® 2003 catalyst, was added to the main beaker at room temperature and mixing continued for approximately 1 minute. The resulting mixture was immediately poured onto a flat surface and allowed to stand for 30 minutes, thereby forming a crosslinked slab. The slab was then reduced to powder by mortar and pestle. The resulting treated particles have an average particle size as measured under a microscope of about 1 micron to 10 microns. Such treated particles contained approximately 85.31 wt% TiO 2 , 3.52% Gantrez S-97BF, 0.41% stannous oct...
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