A kind of rubber core material and preparation method thereof
A rubber core and composite material technology, applied in the field of rubber core material and its preparation, can solve the problems of rubber core material wear resistance and heat resistance need to be improved, cracking on the upper surface, layer-like shedding, etc., to achieve good dimensional stability properties and thermal stability, improve wear resistance and heat resistance, improve toughness and hardness
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Embodiment 1
[0031] The rubber core material of the present embodiment comprises the following components by weight:
[0032]
[0033] The preparation method of the above rubber core material comprises the following steps:
[0034] (1) Preparation of graphene composite material:
[0035] Under ultrasonic conditions, disperse 100 parts of graphene oxide powder in 150 parts of tetrahydrofuran by weight, after graphene oxide forms an amorphous suspension in tetrahydrofuran, add 100 parts of hydrogenated Styrene-butadiene-styrene system mixture, the weight ratio of hydrogenated styrene, butadiene and styrene in the mixture is 1:0.5:1.7;
[0036] After reacting for 1.5h, carry out vacuum distillation, remove the organic solvent and dry to obtain graphene / hydrogenated styrene-butadiene-styrene composite;
[0037] The graphene / hydrogenated styrene-butadiene-styrene composite was melt-blended at 220°C, and the in-situ reduction reaction was carried out for 25 minutes, and the graphene composi...
Embodiment 2
[0043] The rubber core material of the present embodiment comprises the following components by weight:
[0044]
[0045] The preparation method of the above rubber core material comprises the following steps:
[0046] (1) Preparation of graphene composite material:
[0047] Under ultrasonic conditions, disperse 100 parts of graphene oxide powder in 160 parts of tetrahydrofuran by weight, after graphene oxide forms an amorphous suspension in tetrahydrofuran, add 110 parts of hydrogenation powder to the above suspension under stirring conditions. Styrene-butadiene-styrene system mixture, the weight ratio of hydrogenated styrene, butadiene and styrene in the mixture is 1:0.8:1.7;
[0048] After reacting for 1.8h, carry out vacuum distillation, remove the organic solvent and dry to obtain graphene / hydrogenated styrene-butadiene-styrene composite;
[0049] The graphene / hydrogenated styrene-butadiene-styrene composite was melt-blended at 225°C, and the in-situ reduction reacti...
Embodiment 3
[0055] The rubber core material of the present embodiment comprises the following components by weight:
[0056]
[0057] The preparation method of the above rubber core material comprises the following steps:
[0058] (1) Preparation of graphene composite material:
[0059] Under ultrasonic conditions, disperse 100 parts of graphene oxide powder in 180 parts of tetrahydrofuran by weight, after graphene oxide forms an amorphous suspension in tetrahydrofuran, add 120 parts of hydrogenated Styrene-butadiene-styrene system mixture, the weight ratio of hydrogenated styrene, butadiene and styrene in the mixture is 1:0.8:2;
[0060] After reacting for 2 hours, carry out vacuum distillation, remove the organic solvent and dry to obtain graphene / hydrogenated styrene-butadiene-styrene composite;
[0061] Melt and blend the graphene / hydrogenated styrene-butadiene-styrene composite at 230°C, perform an in-situ reduction reaction for 50 minutes, and obtain the graphene composite mate...
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